1YCB

DISTAL POCKET POLARITY IN LIGAND BINDING TO MYOGLOBIN: DEOXY AND CARBONMONOXY FORMS OF A THREONINE68 (E11) MUTANT INVESTIGATED BY X-RAY CRYSTALLOGRAPHY AND INFRARED SPECTROSCOPY

Experimental procedure

Spacegroup name	P 1 21 1
格子定数 [Å]	124.600, 42.500, 92.000
格子定数 [度]	90.00, 92.00, 90.00

精密化法

残基	8.000 - 2.100
R因子	0.198
結合長の平均二乗偏差(RMSD) [Å]	0.020
結合角の平均二乗偏差(RMSD) [度]	0.055
Refinement software	PROLSQ

Quality characteristics

	Overall
分解能 [Å] (高)	2.100 *
Rmerge_l_obs	0.111 *
独立反射数	18251 *

文献の結晶化試薬

ID	結晶ID	溶液	試薬名	濃度 (単位) (単位)	詳細
1	1	drop	sodium phosphate	100 (mM)
2	1	drop	ammonium sulfate	70-80 (%)
3	1	drop	protein	5-6 (mg/ml)
4	1	drop	sodium dithionite		50-fold molar excess