1VYZ
Structure of CDK2 complexed with PNU-181227
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 53.250, 71.910, 72.220 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.430 - 2.210 |
Rwork | 0.238 |
R-free | 0.28000 |
Structure solution method | OTHER |
RMSD bond length | 0.013 |
RMSD bond angle | 1.500 |
Data scaling software | SCALEPACK |
Refinement software | CNX (2002) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.048 | 0.389 |
Number of reflections | 14353 | |
<I/σ(I)> | 14 | 3.3 |
Completeness [%] | 99.5 | 99.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.4 | 10 PERCENT PEG4000, 50 MM AMMONIUN ACETATE, 50 MM HEPES PH 7.4 |