1VYZ

Structure of CDK2 complexed with PNU-181227

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-4
Synchrotron site	ESRF
Beamline	ID14-4
Temperature [K]	100
Spacegroup name	P 21 21 21
格子定数 [Å]	53.250, 71.910, 72.220
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	21.430 - 2.210
Rwork	0.238
R-free	0.28000
Structure solution method	OTHER
結合長の平均二乗偏差(RMSD) [Å]	0.013
結合角の平均二乗偏差(RMSD) [度]	1.500
Data scaling software	SCALEPACK
Refinement software	CNX (2002)

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	30.000	2.280
分解能 [Å] (高)	2.200	2.200
Rmerge_l_obs	0.048	0.389
独立反射数	14353
<I/σ(I)>	14	3.3
完全性 [%]	99.5	99.6

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1		7.4		10 PERCENT PEG4000, 50 MM AMMONIUN ACETATE, 50 MM HEPES PH 7.4