1V07

CRYSTAL STRUCTURE OF ThrE11Val mutant of THE NERVE TISSUE MINI-HEMOGLOBIN FROM THE NEMERTEAN WORM CEREBRATULUS LACTEUS

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Detector technology	CCD
Collection date	2002-12-11
Detector	ADSC CCD
Spacegroup name	P 21 21 21
格子定数 [Å]	42.656, 43.422, 59.660
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	30.000 - 1.700
R因子	0.17025
Rwork	0.167
R-free	0.19526
Structure solution method	OTHER
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	30.000	1.730
分解能 [Å] (高)	1.700	1.700
Rmerge_l_obs	0.073	0.409
独立反射数	12524
<I/σ(I)>	22	5
完全性 [%]	98.3	95.4
冗長性	6.4	5.4

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1		6		AMMONIUM SULFATE, SODIUM ACETATE, PH 6.0