1TLP

CRYSTALLOGRAPHIC STRUCTURAL ANALYSIS OF PHOSPHORAMIDATES AS INHIBITORS AND TRANSITION-STATE ANALOGS OF THERMOLYSIN

Experimental procedure

Spacegroup name	P 61 2 2
格子定数 [Å]	94.100, 94.100, 131.400
格子定数 [度]	90.00, 90.00, 120.00

精密化法

残基	23.300 - 2.300
R因子	0.174
結合長の平均二乗偏差(RMSD) [Å]	0.022
結合角の平均二乗偏差(RMSD) [度]	2.900
Refinement software	TNT

Quality characteristics

	Overall
分解能 [Å] (低)	23.300
分解能 [Å] (高)	2.300
Rmerge_l_obs	NaN *

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	unknown *	7.2 *

文献の結晶化試薬

ID	結晶ID	溶液	試薬名	濃度 (単位) (単位)	詳細
1	1	1	calcium acetate	0.01 (M)
2	1	1	Tris acetate	0.01 (M)
3	1	1	dimethylsulfoxide	7 (%(v/v))