1SNB

STRUCTURE OF SCORPION NEUROTOXIN BMK M8

Experimental procedure

Temperature [K]	293
Detector technology	AREA DETECTOR
Collection date	1991-12-14
Detector	SIEMENS
Spacegroup name	P 1 21 1
格子定数 [Å]	23.320, 38.560, 29.150
格子定数 [度]	90.00, 107.48, 90.00

精密化法

残基	8.000 - 1.900
R因子	0.181
Rwork	0.181
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	AAH II
結合長の平均二乗偏差(RMSD) [Å]	0.016
結合角の平均二乗偏差(RMSD) [度]	26.040 *
Data reduction software	XENGEN
Data scaling software	XENGEN
Phasing software	X-PLOR
Refinement software	X-PLOR

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)		1.950
分解能 [Å] (高)	1.850	1.850
Rmerge_l_obs	0.052	0.118
Total number of observations	6130 *
独立反射数	3802
<I/σ(I)>	10.2	4.59
完全性 [%]	88.4	17.3
冗長性	1.6	1.15

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	Vapor diffusion, sitting drop *	4.55 *

文献の結晶化試薬

ID	結晶ID	溶液	試薬名	濃度 (単位) (単位)	詳細
1	1	drop	protein	20 (mg/ml)
2	1	drop		0.02 (M)
3	1	drop		0.2 (M)