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1RKA

THE APO FORM OF E. COLI RIBOKINASE

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsMAX II BEAMLINE I711
Synchrotron siteMAX II
BeamlineI711
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date1998-05-15
DetectorMARRESEARCH
Spacegroup nameP 31 2 1
格子定数 [Å]61.970, 61.970, 127.834
格子定数 [度]90.00, 90.00, 120.00
精密化法
残基15.000 - 2.300
Rwork0.210
R-free0.25300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1RKD: RESIDUES 4-9 44-93 123-241 AND 254-309.
結合長の平均二乗偏差(RMSD) [Å]0.006

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結合角の平均二乗偏差(RMSD) [度]1.450

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Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareCNS (0.3)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)15.0002.340
分解能 [Å] (高)2.3002.300
Rmerge_l_obs0.0560.235
Total number of observations62741

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独立反射数12644
<I/σ(I)>20.66.7
完全性 [%]96.487.5
冗長性5.55.5
結晶化条件
結晶ID方法pH温度溶液条件
1Vapor diffusion, hanging drop

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4.8drop consists of equal volume of protein and reservoir solutions

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文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11dropribokinase11 (mg/ml)
21dropTris-HCl20 (mM)
31drop0.2 (M)
41reservoirNa acetate0.1 (M)
51reservoirNH4 acetate0.2 (M)
61reservoirmPEG200022-33 (%)

225158

件を2024-09-18に公開中

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