1NGQ
N1G9 (IGG1-LAMBDA) FAB FRAGMENT
Experimental procedure
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY |
Synchrotron site | Photon Factory |
Detector technology | IMAGE PLATE |
Collection date | 1993-10-07 |
Detector | SATOW |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 109.885, 109.885, 97.959 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.400 |
R-factor | 0.194 * |
Rwork | 0.194 |
R-free | 0.25400 |
RMSD bond length | 0.015 |
RMSD bond angle | 0.040 |
Data reduction software | OSC |
Phasing software | X-PLOR (2.1) |
Refinement software | PROLSQ |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 * | |
High resolution limit [Å] | 2.400 | 2.400 * |
Rmerge | 0.075 | |
Total number of observations | 110783 * | |
Number of reflections | 20848 | |
Completeness [%] | 87.0 * | 51 * |
Redundancy | 5.31 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8.5 * | 10 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium salfate | 1.8-1.9 (M) | |
2 | 1 | reservoir | Tris | 0.1 (M) | |
3 | 1 | drop | Fab solution | 10 (mg/ml) | |
4 | 1 | drop | ammonium salfate | 1.8-1.9 (M) | |
5 | 1 | drop | Tris | 0.1 (M) |