1NGP
N1G9 (IGG1-LAMBDA) FAB FRAGMENT COMPLEXED WITH (4-HYDROXY-3-NITROPHENYL) ACETATE
Experimental procedure
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY |
Synchrotron site | Photon Factory |
Detector technology | IMAGE PLATE |
Collection date | 1994-02-22 |
Detector | SATOW |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 110.691, 110.691, 98.250 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.400 |
R-factor | 0.196 * |
Rwork | 0.196 |
R-free | 0.25000 |
RMSD bond length | 0.015 |
RMSD bond angle | 0.039 |
Data reduction software | OSC |
Phasing software | X-PLOR (2.1) |
Refinement software | PROLSQ |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 * | |
High resolution limit [Å] | 2.400 | 2.400 * |
Rmerge | 0.066 | |
Total number of observations | 76319 * | |
Number of reflections | 21761 | |
Completeness [%] | 89.0 * | 68 * |
Redundancy | 3.51 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8.5 * | 10 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium salfate | 1.8-1.9 (M) | |
2 | 1 | reservoir | Tris | 0.1 (M) | |
3 | 1 | drop | Fab solution | 10 (mg/ml) | |
4 | 1 | drop | ammonium salfate | 1.8-1.9 (M) | |
5 | 1 | drop | Tris | 0.1 (M) |