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1N34

Structure of the Thermus thermophilus 30S ribosomal subunit in the presence of codon and crystallographically disordered near-cognate transfer rna anticodon stem-loop mismatched at the first codon position

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-4
Synchrotron siteESRF
BeamlineID14-4
Temperature [K]90
Detector technologyCCD
Collection date2001-05-05
DetectorADSC QUANTUM 4
Spacegroup nameP 41 21 2
格子定数 [Å]401.844, 401.844, 173.854
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基200.000

*

- 3.800
R因子0.241
Rwork0.241
R-free0.31200
Structure solution methodDIFFERENCE FOURIER
Starting model (for MR)1J5E WITHOUT IONS AND PORTIONS AROUND A SITE
結合長の平均二乗偏差(RMSD) [Å]0.007
結合角の平均二乗偏差(RMSD) [度]1.200

*

Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)141.4203.940
分解能 [Å] (高)3.800

*

3.780
Rmerge_l_obs0.080

*

0.295

*

Total number of observations456527

*

独立反射数135995
<I/σ(I)>71.7
完全性 [%]99.3

*

96.1

*

冗長性3.4
結晶化条件
結晶ID方法pH温度溶液条件
1VAPOR DIFFUSION, HANGING DROP6.5277Clemons, W.M., (2001) J. Mol. Biol., 310, 827.

*

結晶化試薬
ID結晶ID濃度試薬名濃度 (単位)詳細
111NH4Cl
1012CaCl2
1112magnesium acetate
1212MPD
211KCl
311CaCl2
411magnesium acetate
511sodium cacodylate
611potassium-MES
711MPD
812NH4Cl
912KCl
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
11reservoirMPD14-16 (%(v/v))
21reservoir0.2 (M)
31reservoir75 (mM)
41reservoir15 (mM)
51reservoirMES0.1 (M)pH6.5

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件を2024-09-18に公開中

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