1MWD
WILD TYPE DEOXY MYOGLOBIN
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 150 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS |
Spacegroup name | I 1 21 1 |
格子定数 [Å] | 122.120, 42.140, 91.490 |
格子定数 [度] | 90.00, 92.85, 90.00 |
精密化法
残基 | 24.000 - 1.800 |
R因子 | 0.196 * |
Rwork | 0.196 |
R-free | 0.24300 |
Structure solution method | OTHER |
結合長の平均二乗偏差(RMSD) [Å] | 0.013 |
結合角の平均二乗偏差(RMSD) [度] | 0.030 |
Data reduction software | DENZO |
Data scaling software | CCP4 |
Phasing software | CCP4 |
Refinement software | REFMAC |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 24.000 | |
分解能 [Å] (高) | 1.800 | |
Rmerge_l_obs | 0.040 * | 0.291 * |
独立反射数 | 42068 | |
<I/σ(I)> | 21.4 | |
完全性 [%] | 96.5 | |
冗長性 | 7.9 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | Vapor diffusion, hanging drop * | 7.1 | 0.1 PHOSPHATE BUFFER 72-80% SATURATED AMMONIUM SULPHATE, pH 7.1 |
文献の結晶化試薬
ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
1 | 1 | drop | ammonium sulfate | 72-80 (%(v/v)sat) | |
2 | 1 | drop | phosphate | 0.1 (M) | |
3 | 1 | drop | protein | 10 (mg/ml) |