1L0A

DOWNSTREAM REGULATOR TANK BINDS TO THE CD40 RECOGNITION SITE ON TRAF3

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL9-1
Synchrotron site	SSRL
Beamline	BL9-1
Temperature [K]	110
Detector technology	IMAGE PLATE
Collection date	2000-12-15
Detector	MARRESEARCH
Wavelength(s)	0.97
Spacegroup name	P 3 2 1
格子定数 [Å]	83.000, 83.000, 76.700
格子定数 [度]	90.00, 90.00, 120.00

精密化法

残基	50.000 - 2.900
R因子	0.23 *
Rwork	0.230
R-free	0.29500
Structure solution method	MOLECULAR REPLACEMENT
結合長の平均二乗偏差(RMSD) [Å]	0.008
結合角の平均二乗偏差(RMSD) [度]	1.420
Data scaling software	CCP4 ((SCALA))
Phasing software	CNS
Refinement software	CNS

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	50.000	2.980
分解能 [Å] (高)	2.900	2.900
Rmerge_l_obs	0.080 *
Total number of observations	38649 *
独立反射数	7263 *
完全性 [%]	99.5	100
冗長性		5.5

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	VAPOR DIFFUSION, HANGING DROP	6.8	298	unpublished data *