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1FQT

CRYSTAL STRUCTURE OF THE RIESKE-TYPE FERREDOXIN ASSOCIATED WITH BIPHENYL DIOXYGENASE

Experimental procedure
Experimental methodMULTIPLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 14-BM-D
Synchrotron siteAPS
Beamline14-BM-D
Temperature [K]100
Detector technologyCCD
Collection date1998-04-10
DetectorADSC QUANTUM 1
Wavelength(s)0.9537,1.742,1.737
Spacegroup nameP 21 21 2
Unit cell lengths76.400, 53.100, 64.700
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution26.000 - 1.600
R-factor0.18
Rwork0.180
R-free0.20000
Structure solution methodFE MAD
RMSD bond length0.011
RMSD bond angle27.200

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Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareMLPHARE
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]26.0001.660
High resolution limit [Å]1.6001.600
Rmerge0.0680.412
Number of reflections34971
<I/σ(I)>9.62.2
Completeness [%]98.997.6
Redundancy4.954.91
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7

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10

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PEG MME 5000, MES buffer, ammonium sulfate, pH 6.3, VAPOR DIFFUSION, SITTING DROP at 283K, pH 6.5
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein31 (mg/ml)
21dropsodium chloride0.15 (M)
31dropdithiothreitol1 (mM)
41dropMOPS20 (mM)
51reservoirmPEG500025 (%)
61reservoirammonium sulfate0.2 (M)
71reservoirMES0.1 (M)

225158

数据于2024-09-18公开中

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