1FM0
MOLYBDOPTERIN SYNTHASE (MOAD/MOAE)
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X26C |
Synchrotron site | NSLS |
Beamline | X26C |
Temperature [K] | 95 |
Detector technology | CCD |
Collection date | 1999-01-01 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | C 1 2 1 |
格子定数 [Å] | 66.029, 48.955, 76.457 |
格子定数 [度] | 90.00, 107.72, 90.00 |
精密化法
残基 | 10.000 - 1.450 |
R因子 | 0.1532 |
Rwork | 0.152 |
R-free | 0.18200 |
結合長の平均二乗偏差(RMSD) [Å] | 0.013 |
結合角の平均二乗偏差(RMSD) [度] | 1.382 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHARP |
Refinement software | REFMAC |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 1.510 |
分解能 [Å] (高) | 1.450 | 1.450 |
Rmerge_l_obs | 0.054 * | 0.454 |
Total number of observations | 426992 * | |
独立反射数 | 43689 | |
<I/σ(I)> | 27.9 | |
完全性 [%] | 95.6 * | 89.5 |
冗長性 | 4.5 | 4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION | 7.5 | 295 | Sodium chloride, Hepes , pH 7.5, VAPOR DIFFUSION, temperature 295K |
文献の結晶化試薬
ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
1 | 1 | reservoir | 5 (M) | ||
2 | 1 | reservoir | HEPES | 0.1 (M) |