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1CQI

Crystal Structure of the Complex of ADP and MG2+ with Dephosphorylated E. Coli Succinyl-CoA Synthetase

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-6A
Synchrotron sitePhoton Factory
BeamlineBL-6A
Temperature [K]283
Detector technologyIMAGE PLATE
Collection date1996-06-08
DetectorFUJI
Spacegroup nameP 43 2 2
格子定数 [Å]99.860, 99.860, 407.150
格子定数 [度]90.00, 90.00, 90.00
精密化法
残基20.000 - 3.300
R因子0.191
Rwork0.191
R-free0.24700
結合長の平均二乗偏差(RMSD) [Å]0.017
結合角の平均二乗偏差(RMSD) [度]25.000

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Data reduction softwareWEIS
Data scaling softwareSCALKB2
Refinement softwareCNS
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)20.0003.500
分解能 [Å] (高)3.3003.300
Rmerge_l_obs0.1640.378
Total number of observations195264

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独立反射数3175315389

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完全性 [%]99.098.4
冗長性6.33.5
結晶化条件
結晶ID方法pH温度溶液条件
1Microdialysis

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7.321

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AMMONIUM SULFATE, POTASSIUM PHOSPHATE, COENZYME A, pH 7.30, VAPOR DIFFUSION, HANGING DROP
文献の結晶化試薬
ID結晶ID溶液試薬名濃度 (単位) (単位)詳細
111ammonium sulfate1.9 (M)
211potassium phosphate0.1 (M)
311dithiothreitol1 (mM)
411CoA0.1 (mM)
511EDTA0.1 (mM)

225158

件を2024-09-18に公開中

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