1CP4

FORMATION, CRYSTAL STRUCTURE, AND REARRANGEMENT OF A CYTOCHROME P450-CAM IRON-PHENYL COMPLEX

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	108.670, 103.900, 36.380
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 * - 1.900
R-factor	0.199
RMSD bond length	0.020
RMSD bond angle	0.036 *
Refinement software	PROFFT

Data quality characteristics

	Overall
High resolution limit [Å]	1.870 *
Rmerge	0.074 *
Total number of observations	128716 *
Completeness [%]	55.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Batch method *		12-15 *	took Poulos et al., 1982 from original paper *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	0.05 (ml)
2	1	1	ammonium sulfate	0.05 (ml)