1B88

V-ALPHA 2.6 MOUSE T CELL RECEPTOR (TCR) DOMAIN

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	1995-06-15
Detector	RIGAKU RAXIS II
Spacegroup name	P 21 21 21
格子定数 [Å]	53.987, 76.187, 88.402
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	10.000 - 2.500
R因子	0.224 *
Rwork	0.224
R-free	0.32400
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1tcr
結合長の平均二乗偏差(RMSD) [Å]	0.007
結合角の平均二乗偏差(RMSD) [度]	26.890 *
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	X-PLOR (3.1)

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	15.000	2.600
分解能 [Å] (高)	2.200	2.500
Rmerge_l_obs	0.127
Total number of observations	174142 *
独立反射数	13408
完全性 [%]	88.8	39.1
冗長性	13

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	unknown *	7		SODIUM FORMATE, pH 7.0, VAPOR DIFFUSION, HANGING DROP

結晶化試薬

ID	結晶ID	濃度	試薬名	濃度 (単位)	詳細
1	1	1	SODIUM FORMATE
2	1	2	SODIUM FORMATE