1AHB
THE N-GLYCOSIDASE MECHANISM OF RIBOSOME-INACTIVATING PROTEINS IMPLIED BY CRYSTAL STRUCTURES OF ALPHA-MOMORCHARIN
Experimental procedure
Spacegroup name | H 3 |
格子定数 [Å] | 131.400, 131.400, 49.800 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 8.000 * - 2.200 |
R因子 | 0.175 |
Rwork | 0.175 |
結合長の平均二乗偏差(RMSD) [Å] | 0.013 |
結合角の平均二乗偏差(RMSD) [度] | 2.890 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 100.000 * | |
分解能 [Å] (高) | 2.200 * | 2.200 * |
Rmerge_l_obs | 0.070 * | 0.094 * |
Total number of observations | 11153 * | |
独立反射数 | 10409 * | 2018 * |
完全性 [%] | 85.8 * | 59.3 * |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | Vapor diffusion, hanging drop * | 7.65 * |
文献の結晶化試薬
ID | 結晶ID | 溶液 | 試薬名 | 濃度 (単位) (単位) | 詳細 |
1 | 1 | drop | 10 (%(w/v)) | ||
2 | 1 | drop | Tris-HCl | 0.05 (M) | |
3 | 1 | drop | protein | 4 (%(w/v)) | |
4 | 1 | reservoir | 23 (%(w/v)) |