196D
CRYSTAL STRUCTURE OF C-T-C-T-C-G-A-G-A-G: IMPLICATIONS FOR THE STRUCTURE OF THE HOLLIDAY JUNCTION
Experimental procedure
Temperature [K] | 93 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS II |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 62.230, 24.320, 40.830 |
Unit cell angles | 90.00, 126.78, 90.00 |
Refinement procedure
Resolution | 8.000 - 1.700 |
R-factor | 0.2 |
RMSD bond length | 0.037 |
RMSD bond angle | 0.045 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.700 |
Rmerge | 0.056 * |
Number of reflections | 4946 |
Completeness [%] | 87.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | standing drop * | 5 * | VAPOR DIFFUSION, SITTING DROP, temperature 278.00K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | CA ACETATE | ||
4 | 1 | 2 | WATER | ||
5 | 1 | 2 | MPD |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA duplex | 1.34 (mM) | |
2 | 1 | drop | calcium acetate | 100-250 (mM) | |
3 | 1 | drop | MPD | 15-19 (%(v/v)) |