151D
DIVERSITY OF WATER RING SIZE AT DNA INTERFACES: HYDRATION AND DYNAMICS OF DNA-ANTHRACYCLINE COMPLEXES
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 113 |
Detector technology | AREA DETECTOR |
Detector | SDMS |
Spacegroup name | P 41 21 2 |
格子定数 [Å] | 27.920, 27.920, 52.390 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | ? - 1.400 |
R因子 | 0.2 |
結合長の平均二乗偏差(RMSD) [Å] | 0.200 * |
結合角の平均二乗偏差(RMSD) [度] | 0.019 * |
Refinement software | NUCLSQ |
Quality characteristics
Overall | |
分解能 [Å] (高) | 1.400 |
Total number of observations | 17251 * |
独立反射数 | 3402 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | pH 6.50, VAPOR DIFFUSION, SITTING DROP |
結晶化試薬
ID | 結晶ID | 濃度 | 試薬名 | 濃度 (単位) | 詳細 |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | NA CACODYLATE | ||
4 | 1 | 1 | MGCL2 | ||
5 | 1 | 1 | SPERMINE_HCL | ||
6 | 1 | 2 | WATER | ||
7 | 1 | 2 | MPD |