108M
SPERM WHALE MYOGLOBIN V68F N-BUTYL ISOCYANIDE AT PH 7.0
Experimental procedure
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 292 |
Detector technology | IMAGE PLATE |
Collection date | 1997-03 |
Detector | RIGAKU |
Spacegroup name | P 6 |
格子定数 [Å] | 91.622, 91.622, 45.984 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 5.000 - 2.670 |
R因子 | 0.124 |
Rwork | 0.124 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | SPERM WHALE MYOGLOBIN 0M D122N (DEOXY) |
結合長の平均二乗偏差(RMSD) [Å] | 0.028 |
結合角の平均二乗偏差(RMSD) [度] | 2.200 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | X-PLOR (3.851) |
Refinement software | X-PLOR (3.851) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 6.000 | 2.680 |
分解能 [Å] (高) | 2.670 | 2.670 |
Rmerge_l_obs | 0.098 | 0.340 |
独立反射数 | 6345 | |
完全性 [%] | 99.0 | 93.9 |
冗長性 | 3.52 | 3.56 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 7 | 3.0 M AMMONIUM SULFATE, 20 MM TRIS, 1MM EDTA, PH 9.0, pH 7.0 |