104M
SPERM WHALE MYOGLOBIN N-BUTYL ISOCYANIDE AT PH 7.0
Experimental procedure
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 292 |
Detector technology | IMAGE PLATE |
Collection date | 1994-03 |
Detector | RIGAKU |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 64.730, 30.910, 34.828 |
格子定数 [度] | 90.00, 105.41, 90.00 |
精密化法
残基 | 5.000 - 1.710 |
R因子 | 0.154 |
Rwork | 0.154 |
R-free | 0.22500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | SPERM WHALE MYOGLOBIN NBNC MINUS LIGAND |
結合長の平均二乗偏差(RMSD) [Å] | 0.009 |
結合角の平均二乗偏差(RMSD) [度] | 1.400 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | X-PLOR (3.851) |
Refinement software | X-PLOR (3.851) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 6.000 | 1.720 |
分解能 [Å] (高) | 1.710 | 1.710 |
Rmerge_l_obs | 0.040 | 0.172 |
独立反射数 | 13484 | |
完全性 [%] | 92.0 | 92.4 |
冗長性 | 3.19 | 3.03 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 7 | 3.0 M AMMONIUM SULFATE, UNBUFFERED, pH 7.0 |