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- PDB-7m54: Crystallographic structure of a cubic crystal form of STMV grown ... -
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Open data
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Basic information
Entry | Database: PDB / ID: 7m54 | ||||||
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Title | Crystallographic structure of a cubic crystal form of STMV grown from bromide | ||||||
![]() | Coat protein | ||||||
![]() | VIRUS | ||||||
Function / homology | Satellite virus coat domain superfamily / viral capsid / structural molecule activity / BROMIDE ION / Coat protein![]() | ||||||
Biological species | ![]() | ||||||
Method | ![]() ![]() ![]() | ||||||
![]() | McPherson, A. | ||||||
![]() | ![]() Title: Structures of additional crystal forms of Satellite tobacco mosaic virus grown from a variety of salts. Authors: McPherson, A. | ||||||
History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 2 MB | Display | ![]() |
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PDB format | ![]() | Display | ![]() | |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Summary document | ![]() | 618.5 KB | Display | ![]() |
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Full document | ![]() | 654.6 KB | Display | |
Data in XML | ![]() | 117.1 KB | Display | |
Data in CIF | ![]() | 157.2 KB | Display | |
Arichive directory | ![]() ![]() | HTTPS FTP |
-Related structure data
Related structure data | ![]() 5bklC ![]() 5bknC ![]() 5bkqC ![]() 7m2tC ![]() 7m2vC ![]() 7m3rC ![]() 7m3tC ![]() 7m50C ![]() 7m57C ![]() 4oq8S S: Starting model for refinement C: citing same article ( |
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Similar structure data |
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Links
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Assembly
Deposited unit | ![]()
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1 | ![]()
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Unit cell |
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Components on special symmetry positions |
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Components
-Protein , 1 types, 20 molecules ABCDEFGHIJKLMNOGGHHIIJJKK
#1: Protein | Mass: 17533.949 Da / Num. of mol.: 20 / Source method: isolated from a natural source / Source: (natural) ![]() |
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-Non-polymers , 5 types, 780 molecules ![](data/chem/img/CA.gif)
![](data/chem/img/BR.gif)
![](data/chem/img/MG.gif)
![](data/chem/img/CL.gif)
![](data/chem/img/HOH.gif)
![](data/chem/img/BR.gif)
![](data/chem/img/MG.gif)
![](data/chem/img/CL.gif)
![](data/chem/img/HOH.gif)
#2: Chemical | ChemComp-CA / #3: Chemical | ChemComp-BR / #4: Chemical | ChemComp-MG / #5: Chemical | #6: Water | ChemComp-HOH / | |
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-Details
Has ligand of interest | Y |
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-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 3.07 Å3/Da / Density % sol: 59.92 % / Description: octahedra |
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Crystal grow | Temperature: 279 K / Method: vapor diffusion, sitting drop / pH: 6 Details: crystals were grown by sitting drop vapor diffusion in Cryschem plates using 0.6 ml reservoirs. Drops were 6 to 8 ul and composed of equal volumes of a 5 mg/ml virus stock solution buffered ...Details: crystals were grown by sitting drop vapor diffusion in Cryschem plates using 0.6 ml reservoirs. Drops were 6 to 8 ul and composed of equal volumes of a 5 mg/ml virus stock solution buffered at pH 6.5 with 0.1M phosphate, and the reservoir solution. The reservoir solution was 18% w/v NaBr buffered with 0.1 M phosphate at pH 6.0. Crystallization was carried out at 4 degrees C. PH range: 4.5 - 7.0 |
-Data collection
Diffraction | Mean temperature: 173 K / Serial crystal experiment: N |
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Diffraction source | Source: ![]() ![]() ![]() |
Detector | Type: MAR CCD 165 mm / Detector: CCD / Date: Jun 21, 2002 |
Radiation | Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Wavelength: 1 Å / Relative weight: 1 |
Reflection | Resolution: 3.5→105 Å / Num. obs: 38017 / % possible obs: 73 % / Redundancy: 4.6 % / Biso Wilson estimate: 50.24 Å2 / CC1/2: 0.94 / Rmerge(I) obs: 0.21 / Rsym value: 0.2 / Net I/σ(I): 7.7 |
Reflection shell | Resolution: 3.5→3.65 Å / Rmerge(I) obs: 0.32 / Mean I/σ(I) obs: 1.1 / Num. unique obs: 1200 / CC1/2: 0.32 / Rsym value: 0.3 |
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Processing
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Refinement | Method to determine structure: ![]() Starting model: 4OQ8 Resolution: 3.8→56.91 Å / SU ML: 0.5762 / Cross valid method: FREE R-VALUE / σ(F): 1.33 / Phase error: 36.6351 Stereochemistry target values: GeoStd + Monomer Library + CDL v1.2
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Solvent computation | Shrinkage radii: 0.9 Å / VDW probe radii: 1.11 Å / Solvent model: FLAT BULK SOLVENT MODEL | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Displacement parameters | Biso mean: 85.34 Å2 | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Refinement step | Cycle: LAST / Resolution: 3.8→56.91 Å
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Refine LS restraints |
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LS refinement shell |
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Refinement TLS params. | Method: refined / Origin x: 88.363990023 Å / Origin y: 174.697357596 Å / Origin z: 27.1460215295 Å
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Refinement TLS group | Selection details: all |