温度: 298 K / 手法: 蒸気拡散法, ハンギングドロップ法 / pH: 7 詳細: Crystallization drops were prepared by mixing 2 uL of stock peptide solution with 2 uL of mother liquor and allowed to equilibrate at 298 K over a well containing 500 uL of mother liquor. The ...詳細: Crystallization drops were prepared by mixing 2 uL of stock peptide solution with 2 uL of mother liquor and allowed to equilibrate at 298 K over a well containing 500 uL of mother liquor. The stock peptide solution (total concentration 1.5 mM) was prepared by mixing 2:1 ratios of the A16 peptide with IPF-F16 in 10 mM potassium phosphate, 100 mM potassium chloride pH 7.0.
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データ収集
回折
平均測定温度: 100 K / Serial crystal experiment: N
放射光源
由来: シンクロトロン / サイト: ALS / ビームライン: 4.2.2 / 波長: 0.83 Å
検出器
タイプ: RDI CMOS_8M / 検出器: CMOS / 日付: 2018年1月9日
放射
プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
放射波長
波長: 0.83 Å / 相対比: 1
反射
解像度: 2.2→19.85 Å / Num. obs: 8716 / % possible obs: 97.92 % / 冗長度: 1.8 % / Biso Wilson estimate: 34.53 Å2 / CC1/2: 0.986 / CC star: 0.997 / Rmerge(I) obs: 0.07098 / Rpim(I) all: 0.07098 / Rrim(I) all: 0.1004 / Net I/σ(I): 14.32