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- PDB-6tge: NADP dependent methylene-tetrahydromethanopterin dehydrogenase-NA... -

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Basic information

Entry
Database: PDB / ID: 6tge
TitleNADP dependent methylene-tetrahydromethanopterin dehydrogenase-NADP+-methenyl-H4MPT+ complex
ComponentsBifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
KeywordsOXIDOREDUCTASE / dehydrogenase / tetrahydromethanotperin / NADP / methyotrophic bacteria / energy metabolism
Function / homology
Function and homology information


Oxidoreductases; Acting on the CH-NH group of donors; With NAD+ or NADP+ as acceptor / methylenetetrahydrofolate dehydrogenase (NADP+) / methylenetetrahydrofolate dehydrogenase (NADP+) activity / formaldehyde catabolic process / one-carbon metabolic process / oxidoreductase activity / cytoplasm
Similarity search - Function
Methylene-tetrahydromethanopterin dehydrogenase, N-terminal domain / Methylene-tetrahydromethanopterin dehydrogenase, N-terminal / Methylene tetrahydromethanopterin dehydrogenase, NADP-binding domain / Methylene-tetrahydromethanopterin dehydrogenase, N-terminal domain superfamily / Methylene-tetrahydromethanopterin dehydrogenase, N-terminal / Aminoacid dehydrogenase-like, N-terminal domain superfamily / NAD(P)-binding Rossmann-like Domain / NAD(P)-binding domain superfamily / Rossmann fold / 3-Layer(aba) Sandwich / Alpha Beta
Similarity search - Domain/homology
5,10-DIMETHYLENE TETRAHYDROMETHANOPTERIN / NADP NICOTINAMIDE-ADENINE-DINUCLEOTIDE PHOSPHATE / NADP-dependent methylenetetrahydromethanopterin/methylenetetrahydrofolat e dehydrogenase / Bifunctional protein MdtA
Similarity search - Component
Biological speciesMethylorubrum extorquens (bacteria)
MethodX-RAY DIFFRACTION / SYNCHROTRON / MOLECULAR REPLACEMENT / Resolution: 1.5 Å
AuthorsErmler, U. / Shima, S.
CitationJournal: J.Mol.Biol. / Year: 2020
Title: The Hydride Transfer Process in NADP-dependent Methylene-tetrahydromethanopterin Dehydrogenase.
Authors: Huang, G. / Wagner, T. / Demmer, U. / Warkentin, E. / Ermler, U. / Shima, S.
History
DepositionNov 15, 2019Deposition site: PDBE / Processing site: PDBE
Revision 1.0Feb 26, 2020Provider: repository / Type: Initial release
Revision 1.1May 20, 2020Group: Database references / Category: citation
Item: _citation.journal_volume / _citation.page_first ..._citation.journal_volume / _citation.page_first / _citation.page_last / _citation.title
Revision 1.2Jan 24, 2024Group: Advisory / Data collection ...Advisory / Data collection / Database references / Refinement description
Category: chem_comp_atom / chem_comp_bond ...chem_comp_atom / chem_comp_bond / database_2 / pdbx_initial_refinement_model / pdbx_unobs_or_zero_occ_atoms
Item: _database_2.pdbx_DOI / _database_2.pdbx_database_accession

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Structure visualization

Structure viewerMolecule:
MolmilJmol/JSmol

Downloads & links

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Assembly

Deposited unit
A: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
B: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
C: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
D: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
E: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
F: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
G: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
H: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
I: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
J: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
K: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
L: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
M: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
N: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
O: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
P: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
Q: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
R: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
S: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
T: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
U: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
V: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
W: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
X: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
hetero molecules


Theoretical massNumber of molelcules
Total (without water)752,06280
Polymers714,52324
Non-polymers37,53956
Water138,4277684
1
A: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
B: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
C: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
hetero molecules


Theoretical massNumber of molelcules
Total (without water)94,00810
Polymers89,3153
Non-polymers4,6927
Water543
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
Buried area10910 Å2
ΔGint-54 kcal/mol
Surface area30960 Å2
MethodPISA
2
D: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
E: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
F: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
hetero molecules


Theoretical massNumber of molelcules
Total (without water)94,00810
Polymers89,3153
Non-polymers4,6927
Water543
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
Buried area11040 Å2
ΔGint-58 kcal/mol
Surface area30610 Å2
MethodPISA
3
G: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
H: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
I: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
hetero molecules


Theoretical massNumber of molelcules
Total (without water)94,00810
Polymers89,3153
Non-polymers4,6927
Water543
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
Buried area11240 Å2
ΔGint-60 kcal/mol
Surface area30560 Å2
MethodPISA
4
J: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
K: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
L: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
hetero molecules


Theoretical massNumber of molelcules
Total (without water)94,00810
Polymers89,3153
Non-polymers4,6927
Water543
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
Buried area11070 Å2
ΔGint-57 kcal/mol
Surface area30790 Å2
MethodPISA
5
M: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
N: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
O: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
hetero molecules


Theoretical massNumber of molelcules
Total (without water)94,00810
Polymers89,3153
Non-polymers4,6927
Water543
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
Buried area11070 Å2
ΔGint-58 kcal/mol
Surface area30890 Å2
MethodPISA
6
P: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
Q: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
R: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
hetero molecules


Theoretical massNumber of molelcules
Total (without water)94,00810
Polymers89,3153
Non-polymers4,6927
Water543
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
Buried area11090 Å2
ΔGint-60 kcal/mol
Surface area30790 Å2
MethodPISA
7
S: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
T: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
U: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
hetero molecules


Theoretical massNumber of molelcules
Total (without water)94,00810
Polymers89,3153
Non-polymers4,6927
Water543
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
Buried area10830 Å2
ΔGint-59 kcal/mol
Surface area30810 Å2
MethodPISA
8
V: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
W: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
X: Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase
hetero molecules


Theoretical massNumber of molelcules
Total (without water)94,00810
Polymers89,3153
Non-polymers4,6927
Water543
TypeNameSymmetry operationNumber
identity operation1_555x,y,z1
Buried area11190 Å2
ΔGint-67 kcal/mol
Surface area30560 Å2
MethodPISA
Unit cell
Length a, b, c (Å)98.640, 123.500, 167.300
Angle α, β, γ (deg.)94.790, 100.390, 108.970
Int Tables number1
Space group name H-MP1

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Components

#1: Protein ...
Bifunctional NADP-dependent methylenetetrahydromethanopterin dehydrogenase/methylenetetrahydrofolate dehydrogenase / NADP-dependent methylenetetrahydromethanopterin/methylenetetrahydrofolat e dehydrogenase


Mass: 29771.807 Da / Num. of mol.: 24
Source method: isolated from a genetically manipulated source
Source: (gene. exp.) Methylorubrum extorquens (bacteria) / Gene: mtdA, BV511_24355, TK0001_4179
Production host: Escherichia coli 'BL21-Gold(DE3)pLysS AG' (bacteria)
References: UniProt: A0A1P8QVR4, UniProt: P55818*PLUS, Oxidoreductases; Acting on the CH-NH group of donors; With NAD+ or NADP+ as acceptor
#2: Chemical...
ChemComp-NAP / NADP NICOTINAMIDE-ADENINE-DINUCLEOTIDE PHOSPHATE / 2'-MONOPHOSPHOADENOSINE 5'-DIPHOSPHORIBOSE


Mass: 743.405 Da / Num. of mol.: 24 / Source method: obtained synthetically / Formula: C21H28N7O17P3 / Feature type: SUBJECT OF INVESTIGATION
#3: Chemical...
ChemComp-H4M / 5,10-DIMETHYLENE TETRAHYDROMETHANOPTERIN


Mass: 788.693 Da / Num. of mol.: 24 / Source method: obtained synthetically / Formula: C31H45N6O16P / Feature type: SUBJECT OF INVESTIGATION
#4: Chemical
ChemComp-SO4 / SULFATE ION


Mass: 96.063 Da / Num. of mol.: 8 / Source method: obtained synthetically / Formula: SO4
#5: Water ChemComp-HOH / water


Mass: 18.015 Da / Num. of mol.: 7684 / Source method: isolated from a natural source / Formula: H2O
Has ligand of interestY

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Experimental details

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Experiment

ExperimentMethod: X-RAY DIFFRACTION / Number of used crystals: 1

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Sample preparation

CrystalDensity Matthews: 2.62 Å3/Da / Density % sol: 53.09 %
Crystal growTemperature: 293 K / Method: vapor diffusion / pH: 8
Details: 22% PEG4000, 0.2 M ammonium sulfate, 0.1 M sodium acetate

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Data collection

DiffractionMean temperature: 100 K / Serial crystal experiment: N
Diffraction sourceSource: SYNCHROTRON / Site: SLS / Beamline: X10SA / Wavelength: 1 Å
DetectorType: DECTRIS PILATUS 2M / Detector: PIXEL / Date: Nov 28, 2010
RadiationProtocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelengthWavelength: 1 Å / Relative weight: 1
ReflectionResolution: 1.5→50 Å / Num. obs: 1110526 / % possible obs: 95.5 % / Redundancy: 3.9 % / CC1/2: 0.999 / Net I/σ(I): 9.6
Reflection shellResolution: 1.5→1.6 Å / Num. unique obs: 191566 / CC1/2: 0.574

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Processing

Software
NameVersionClassification
PHENIX1.14_3260refinement
PDB_EXTRACT3.25data extraction
XDSdata reduction
XSCALEdata scaling
PHASERphasing
RefinementMethod to determine structure: MOLECULAR REPLACEMENT
Starting model: 1LU9

1lu9


Resolution: 1.5→48.761 Å / SU ML: 0.23 / Cross valid method: THROUGHOUT / σ(F): 1.92 / Phase error: 30.29 / Stereochemistry target values: ML
RfactorNum. reflection% reflection
Rfree0.2163 55322 4.99 %
Rwork0.1856 1053971 -
obs0.1871 1109293 95.41 %
Solvent computationShrinkage radii: 0.9 Å / VDW probe radii: 1.11 Å / Solvent model: FLAT BULK SOLVENT MODEL
Displacement parametersBiso max: 115.18 Å2 / Biso mean: 31.2138 Å2 / Biso min: 12.44 Å2
Refinement stepCycle: final / Resolution: 1.5→48.761 Å
ProteinNucleic acidLigandSolventTotal
Num. atoms50016 0 2099 7743 59858
Biso mean--37.98 37.51 -
Num. residues----6888
LS refinement shell

Refine-ID: X-RAY DIFFRACTION / Rfactor Rfree error: 0

Resolution (Å)Rfactor RfreeNum. reflection RfreeRfactor RworkNum. reflection Rwork% reflection obs (%)
1.5-1.5170.446418020.43573393892
1.517-1.53490.436717950.40183455394
1.5349-1.55360.406217620.38633450194
1.5536-1.57330.385518800.36723456394
1.5733-1.5940.378718260.35013459394
1.594-1.61580.352417910.33463455394
1.6158-1.63890.35218330.31843468694
1.6389-1.66340.339318550.30523483795
1.6634-1.68930.335117920.29243494195
1.6893-1.7170.313417480.27653504695
1.717-1.74670.302518470.26693494895
1.7467-1.77840.278618200.25363507395
1.7784-1.81260.269518870.24393506695
1.8126-1.84960.275718390.2383514495
1.8496-1.88980.271218320.22833510095
1.8898-1.93380.246618370.21083521695
1.9338-1.98220.241417920.19563528296
1.9822-2.03580.225318630.18963541196
2.0358-2.09570.233218690.18513540296
2.0957-2.16330.215118480.17513541296
2.1633-2.24060.203518550.17113559596
2.2406-2.33030.203218480.16393553997
2.3303-2.43640.196818890.16533536696
2.4364-2.56480.202618780.16133563597
2.5648-2.72550.199319290.15773577497
2.7255-2.93590.201318950.16213572197
2.9359-3.23130.183618850.15653568797
3.2313-3.69880.179418390.14963499695
3.6988-4.65950.154819090.1333592098
4.6595-48.750.178318770.16453547396
Refinement TLS params.

Method: refined / Refine-ID: X-RAY DIFFRACTION

IDL11 (°2)L12 (°2)L13 (°2)L22 (°2)L23 (°2)L33 (°2)S11 (Å °)S12 (Å °)S13 (Å °)S21 (Å °)S22 (Å °)S23 (Å °)S31 (Å °)S32 (Å °)S33 (Å °)T11 (Å2)T12 (Å2)T13 (Å2)T22 (Å2)T23 (Å2)T33 (Å2)Origin x (Å)Origin y (Å)Origin z (Å)
13.2310.3280.29295.0931-0.27070.7545-0.0471-0.0169-0.2179-0.10960.0382-0.02760.0866-0.04390.00020.17050.01660.02520.15820.0010.088619.37811.97871.4386
22.40862.1056-0.42113.8645-0.3550.7976-0.0921-0.0429-0.2923-0.04620.0322-0.34940.10410.02350.10130.18350.06140.00350.14760.00150.168835.207218.861771.238
33.5406-0.7667-0.65584.81342.35125.0078-0.0096-0.2463-0.09170.29180.0771-0.4120.05420.0755-0.06750.16560.0282-0.05270.15970.01370.198442.776926.718679.2619
43.98061.46320.39472.95410.58881.7314-0.13030.03160.3197-0.09960.0548-0.1455-0.12130.03380.02650.20950.0324-0.0110.11270.0070.219639.028841.722469.7706
55.24144.60840.82674.04360.73330.1429-0.28560.24980.051-0.49440.24560.1306-0.0059-0.06220.05410.24370.0070.01170.20770.00480.086826.98722.919861.5959
64.66313.92-0.79893.8996-1.06370.7386-0.30850.1603-0.4969-0.32760.1662-0.49310.1187-0.07510.06120.25460.01930.0670.1686-0.04140.199434.602915.737562.1934
71.5262-0.1832-0.36080.74480.15380.251-0.07420.0275-0.00630.06720.04410.30510.0181-0.108-0.00880.25940.01750.01380.19910.02160.1786-1.13058.387776.6649
80.6587-0.0066-0.06290.437-0.16140.88740.0308-0.0701-0.19420.1156-0.0024-0.0110.04130.0306-0.07820.24290.01110.00940.1850.01830.23826.4106-19.507485.8506
90.51770.3550.11640.8484-0.03830.35880.00220.0459-0.1295-0.04940.01140.03450.00720.070.01170.23330.00740.01660.196-0.01110.21757.5532-12.535172.6163
100.60430.1310.22920.6341-0.05850.131-0.07230.02070.2378-0.0360.07080.048-0.0536-0.0026-0.02910.24840.0232-0.02140.2010.01370.20948.131930.049772.1917
110.8627-0.149-0.50041.28280.23981.47370.0382-0.09960.1630.2231-0.05320.3934-0.0231-0.1957-0.00830.26440.01520.02850.2386-0.00380.4432-18.848741.189281.1633
120.44760.06220.20910.06690.10210.2963-0.09190.1888-0.01260.0567-0.01030.2990.1673-0.2456-0.0750.276-0.0116-0.01210.26210.01870.4481-19.050229.392772.1351
130.9561-0.0423-0.32710.1766-0.07360.2950.00080.40170.1508-0.2969-0.08450.1358-0.0782-0.0975-0.02010.24750.0327-0.04540.21250.050.3168-4.403437.989865.0982
140.67120.0068-0.97080.50740.00133.0096-0.00430.0844-0.16580.0859-0.0163-0.04450.05780.1229-0.23160.164-0.0137-0.00050.1227-0.01080.15339.0105-23.49935.6557
150.3958-0.2322-0.10810.6408-0.090.25730.02620.064-0.40650.07650.0119-0.07350.10190.0312-0.11720.2095-0.00960.00380.1712-0.03680.314444.4841-33.591934.0052
160.6388-0.6820.24011.2836-0.0590.23250.02140.2167-0.7352-0.0614-0.00140.06840.0701-0.03440.08910.211-0.04480.02990.2275-0.09320.475118.498-38.322328.6477
170.1386-0.18440.02260.28240.02240.0710.10350.2697-0.3228-0.16030.0875-0.16120.1004-0.00560.59720.1955-0.06420.05290.2027-0.49160.461322.5397-39.469117.8769
180.3009-0.09270.07680.16980.01790.11240.00230.1018-0.19340.0838-0.04310.3371-0.0141-0.1843-0.01930.1865-0.02670.03040.2252-0.06040.34837.4527-30.963429.4975
190.86941.5253-0.66753.1353-1.20231.316-0.0452-0.2068-0.07470.2227-0.00120.1606-0.0104-0.2014-0.08310.2134-0.03190.05350.1286-0.00670.152627.2982-30.393642.4867
200.112-0.2630.16150.8147-0.16230.51290.0741-0.0743-0.19880.22190.0141-0.00150.1062-0.0788-0.12320.2358-0.03520.03370.1470.06380.441430.9876-40.046240.4248
210.311-0.05420.08850.18730.10740.12270.0060.00160.07060.06530.0176-0.07-0.1577-0.02920.03280.18160.0022-0.00530.1487-0.01820.133550.9977-14.659236.8462
221.5632-0.3101-0.34150.4197-0.06750.41760.0140.01720.3080.00990.0484-0.2328-0.09870.08920.01890.1818-0.0057-0.0130.1282-0.01630.220557.1032-4.840337.6261
231.2344-0.742-0.37580.9703-0.38931.0619-0.1209-0.0613-0.02440.07590.0562-0.2582-0.07820.1514-0.11780.1576-0.0068-0.03680.156-0.03620.266876.5421-24.311237.2102
240.1147-0.0493-0.03650.2269-0.12820.12290.04790.14910.0055-0.02360.0535-0.3145-0.07920.16090.12030.1672-0.0176-0.00590.1692-0.02960.275778.3263-21.184830.2315
250.1051-0.02940.10480.0481-0.06570.13910.00430.2580.114-0.2024-0.0784-0.083-0.1803-0.03270.14510.2339-0.04520.02980.2357-0.03190.315579.7099-17.390224.2693
261.5452-0.71330.97770.4561-0.53150.6662-0.14950.2046-0.1781-0.1033-0.0355-0.16280.20540.19070.29750.1563-0.00950.0030.2202-0.04730.330484.0613-32.228328.568
271.6118-1.03210.01411.483-0.21940.49620.0075-0.0309-0.1498-0.0046-0.0062-0.20630.08460.0486-0.01730.15240.0037-0.01220.1609-0.03050.349280.2002-37.235930.5491
282.47210.911.06510.42540.51160.72060.0456-0.1422-0.42370.11530.0579-0.18090.21290.00020.08530.20770.0188-0.03570.1771-0.00370.341974.1915-37.446837.2081
290.0286-0.05890.07010.2586-0.44470.8617-0.0752-0.2456-0.11740.15790.1026-0.13980.0470.08240.02820.1807-0.0051-0.02360.1601-0.02880.219762.1551-22.457544.1252
301.5963-0.19740.05940.13220.00260.0462-0.0967-0.29990.09680.22780.0584-0.1306-0.04390.1128-0.00810.22230.0043-0.04890.1754-0.040.221868.1357-14.072544.9904
310.817-0.06470.05590.58570.22310.9003-0.0156-0.01180.01140.0185-0.03560.19970.0144-0.1371-0.00120.1714-0.01490.01760.1247-0.01950.139730.5534-8.524236.7985
320.6070.4283-0.0821.24150.0660.6614-0.04620.09980.1628-0.12090.08790.1896-0.0597-0.0012-0.03510.1687-0.01420.01660.13570.00190.17635.195417.836738.2962
330.2927-0.0404-0.08190.2695-0.20990.2862-0.04860.0128-0.0945-0.03230.0361-0.06890.1177-0.0395-0.12570.19440.01130.00920.18370.01490.18487.2279-49.1738152.8699
340.89570.59690.19240.80070.00680.2142-0.05030.0893-0.2868-0.10360.0615-0.2120.09040.06940.04530.19340.02480.02440.1686-0.00190.244394.344-58.3004153.491
350.61590.0259-0.03650.68610.17280.567-0.0533-0.01060.09860.00940.0961-0.3157-0.01870.1010.0180.14940.02-0.00630.1738-0.00610.3298111.1341-32.9774155.5096
360.57240.04030.62420.19430.00941.318-0.10670.20740.3059-0.27680.0325-0.1017-0.34580.06230.07170.2368-0.02520.00480.15440.04230.3362104.4865-24.1338145.9849
370.47040.19510.75880.94840.40271.3019-0.08610.23040.1201-0.27430.01210.10160.00790.0181-0.14860.1886-0.00340.02280.23950.02160.201396.0974-42.4069142.4214
380.9336-1.10980.68992.3481-1.77961.859-0.15090.3579-0.1882-0.26130.0416-0.17740.10140.1407-0.15710.19750.00480.08240.2214-0.0330.2117103.6256-49.6884143.1578
391.1507-0.1743-0.11940.62830.15050.2542-0.04050.03070.01590.010.03210.27620.0199-0.0901-0.03530.16330.02270.00550.14330.02170.223567.8705-56.814157.5458
400.7502-0.017-0.02551.1384-0.28240.80050.0220.0167-0.1147-0.0693-0.01260.03920.00530.00550.00760.0940.00660.00630.108-0.00260.173475.9243-82.1958161.9251
410.97920.05660.17810.6782-0.11820.1603-0.02440.03740.235-0.05070.0304-0.0053-0.03580.0085-0.14010.19650.0209-0.00250.17990.02570.263777.1755-35.2018153.0252
420.53670.11640.20190.58340.16350.50110.0279-0.07210.04470.1803-0.06890.38510.0376-0.15970.0440.2270.01510.04870.19420.02390.465350.2162-24.0357162.1935
431.1637-0.0113-0.37070.64330.0340.6715-0.01510.1634-0.07410.0416-0.05790.42830.1805-0.2241-0.08840.144-0.0125-0.01470.14480.02630.430449.9363-35.8575153.1311
440.96420.02770.17960.0437-0.01220.10230.08350.40140.106-0.2472-0.105-0.1052-0.1248-0.0178-0.10980.21960.0369-0.0370.21260.0580.333364.5854-27.2232146.0373
450.93610.10090.01110.4873-0.03550.4029-0.0449-0.00020.1351-0.05710.01280.1394-0.0613-0.0263-0.01850.25720.0353-0.0340.1876-0.01010.199747.9495-25.660470.9407
460.8454-0.0844-0.19780.03090.03940.1288-0.0055-0.0054-0.0089-0.1965-0.03890.22130.1145-0.38290.010.28580.0378-0.05030.2470.00610.330126.1551-43.934569.8103
470.21810.26620.05870.75660.29410.2368-0.0063-0.1554-0.0190.17410.03250.30490.037-0.05070.11140.26850.05180.00130.2396-0.00780.321829.3556-39.210478.5747
480.1980.2604-0.11380.8075-0.18060.3311-0.07260.0913-0.2434-0.12020.05090.0450.0886-0.0857-0.0180.28430.0278-0.00520.2281-0.0320.348933.105-54.206669.0597
490.83110.9646-0.72671.2251-0.68710.8835-0.16810.2597-0.1696-0.28550.0307-0.00340.1493-0.0025-0.05930.27440.007-0.04840.2529-0.0180.240345.2838-35.382460.9576
501.99331.693-1.21031.7074-1.26290.9341-0.30430.26650.1862-0.30530.11040.0035-0.01840.02110.00040.24920.0313-0.08130.21780.00740.216537.7261-28.166361.5818
510.7114-0.01990.07570.6705-0.04080.1979-0.0351-0.00240.00860.04010.0467-0.2232-0.05710.1101-0.05210.27950.032-0.02310.2207-0.01940.194673.2801-21.005276.525
520.6644-0.03150.05560.78190.24380.90180.0024-0.07870.19190.01270.03240.0484-0.018-0.0631-0.01510.21590.0236-0.01240.1947-0.01360.234963.59217.306483.9613
530.03240.0962-0.00620.60770.2310.16980.0060.03830.1082-0.13270.0274-0.2299-0.03010.01980.10240.3080.0197-0.00970.23810.00420.251571.4962-6.521870.349
540.90030.5074-0.25311.1946-0.08350.2639-0.06780.0221-0.2769-0.04030.0544-0.04910.057-0.01950.02670.29280.03380.00830.2335-0.02760.295264.0696-42.628771.8463
550.7870.4929-0.18590.8333-0.29730.73690.0331-0.0648-0.14070.358-0.0869-0.517-0.06410.08750.04820.29510.0096-0.10550.1636-0.02140.470191.1692-53.595381.6759
560.2323-0.15510.07381.0738-0.1090.59940.01440.183-0.09450.0608-0.0105-0.4267-0.11290.2221-0.03120.2399-0.00070.01240.1803-0.03940.377986.9706-44.592470.1394
570.74840.24350.1780.650.24040.434-0.0074-0.05980.16790.0046-0.01580.0147-0.09310.03760.06720.14860.03090.00260.12910.00230.177276.834125.9078151.9031
580.93880.13240.08430.8941-0.09490.5596-0.02070.0132-0.1685-0.06120.03260.13780.0554-0.0339-0.00650.1340.03290.0030.11750.00780.194962.36847.8139150.8431
590.69050.02310.36850.8029-0.12870.2482-0.0146-0.0092-0.00380.08130.0396-0.1513-0.05080.07510.10390.180.0244-0.00670.1771-0.02220.2366102.187330.5233157.4881
600.53580.02270.21040.6575-0.02311.0771-0.0064-0.11790.26580.07210.0310.0004-0.0407-0.0254-0.0190.13460.0153-0.00390.1607-0.03790.313494.611358.4844167.1844
611.66230.1931-0.60630.38630.23090.86430.03070.09250.0794-0.1052-0.010.0488-0.0201-0.0692-0.0430.1880.0092-0.01650.18590.00720.27593.732651.5318153.7981
620.31690.17880.0721.0927-0.30521.32110.0001-0.017-0.12670.01390.0618-0.08080.0611-0.057-0.00880.19560.0315-0.01110.2023-0.01040.227395.554214.9787153.3554
630.89270.2258-0.39690.5416-0.11430.1848-0.05650.0102-0.3874-0.02630.0632-0.0209-0.0049-0.03730.29990.19450.033-0.00720.1888-0.01620.323791.01114.4563151.9959
640.6878-0.0581-0.2740.5492-0.17450.45370.00720.045-0.12970.1575-0.0632-0.4726-0.04750.05330.02390.17810.0155-0.06340.156-0.0070.5122116.9043-1.8608158.307
650.26040.175-0.08780.66570.02740.77990.0597-0.1539-0.22140.3956-0.1153-0.7759-0.04180.6436-0.00850.1204-0.016-0.21550.10760.03250.7122123.78731.5129162.7122
661.22850.1980.69770.4268-0.13320.7665-0.01370.2506-0.1593-0.0745-0.0328-0.33340.00210.1128-0.13570.20170.03350.02790.2166-0.04720.3876107.19995.5314146.7837
670.34660.09570.02950.40990.32291.12160.093-0.03760.0630.17190.0047-0.16790.0597-0.102-0.03470.2455-0.0234-0.04270.20040.01720.255891.90146.952336.3944
680.8068-0.26020.05680.8237-0.0330.23020.0451-0.03170.29140.15850.001-0.0573-0.02-0.02750.03960.1928-0.0209-0.00420.16170.00610.273891.675857.449534.9248
690.0611-0.0560.20450.1278-0.30390.8225-0.0854-0.02740.15280.0317-0.0762-0.2197-0.17790.1054-0.27430.2024-0.00670.04690.1905-0.07570.5937117.381464.794229.545
701.20570.61540.44431.6605-0.34270.6745-0.10170.2732-0.0316-0.55860.0929-0.4369-0.07620.07560.01030.1769-0.01190.08240.1601-0.04310.3715111.739961.68225.9619
711.2346-0.59670.19830.2988-0.09650.0572-0.01940.4613-0.1799-0.45290.0594-0.24270.11610.0711-0.00920.2635-0.0290.12410.2172-0.02670.3523109.241562.387419.2956
720.2584-0.25770.18270.2507-0.18110.13090.07040.3127-0.0127-0.2503-0.0936-0.4205-0.0590.1094-0.16420.1994-0.00190.0890.2698-0.06960.6211124.00858.429624.552
730.8099-0.2474-0.26140.08880.00160.5643-0.0382-0.02780.0414-0.0199-0.0429-0.19510.04550.2305-0.38850.11080.04160.00950.2202-0.09040.7252125.586953.878529.3256
740.3212-0.0034-0.29560.0222-0.04780.3713-0.0877-0.3270.02480.1051-0.0495-0.2924-0.00410.2663-0.24250.02170.0544-0.12550.2258-0.0310.7482122.414652.490737.5011
751.5714-0.1391-0.18130.0147-0.00021.3070.0063-0.1168-0.19850.348-0.0696-0.1580.00380.0743-0.03610.2385-0.0389-0.12040.1766-0.00850.342103.250553.958443.7723
760.4323-0.0758-0.60590.5094-0.04040.90540.1725-0.20720.35090.3125-0.0893-0.0731-0.11410.1337-0.35790.2167-0.0482-0.02160.1581-0.03850.302599.729563.5641.4408
770.7947-0.3592-0.02590.801-0.16790.46040.0879-0.0517-0.20990.1714-0.05560.02010.1388-0.019-0.12520.2342-0.0294-0.02940.14660.03330.165176.445332.441237.4543
780.84660.161-0.16530.50880.11890.5436-0.00360.04190.07690.01960.00790.2910.0493-0.16760.04560.2046-0.02570.04370.20370.01180.290452.234146.359129.3501
790.96520.25740.14460.48510.08960.47020.0091-0.14780.1470.2302-0.01010.2108-0.0858-0.08110.0350.2603-0.02380.06580.2035-0.01250.256659.26652.182938.3453
801.1199-0.36760.15680.7343-0.04081.34440.0628-0.0654-0.08710.2473-0.0038-0.53960.10690.07310.07280.2497-0.0095-0.13540.14740.03220.3731100.322132.057438.1812
811.0856-0.0517-0.43640.6748-0.26170.4677-0.12260.2214-0.58870.09080.0351-1.06880.14380.0059-0.06190.2509-0.0116-0.14320.17510.01740.653197.48531.525335.9315
820.6834-0.3460.06350.59630.63991.07290.1067-0.0465-0.14750.9155-0.2106-0.10060.1407-0.1121-0.32340.4486-0.0332-0.21420.1490.08930.328993.104511.788446.3642
830.4064-0-0.17141.54630.12860.3584-0.08450.0619-0.35210.10990.04850.2160.0830.03120.02140.3263-0.01370.07190.2518-0.00260.47641.902610.7185116.6852
840.66680.85661.02772.60871.46672.4020.0377-0.1238-0.13690.1337-0.04770.31690.0339-0.11630.36530.26950.00030.09240.2184-0.00880.717920.53434.3831117.4338
850.82991.0730.27711.83060.31861.2894-0.05420.1108-0.3432-0.20510.07530.20060.12340.00280.04580.3213-0.02170.0060.3274-0.12120.857617.23750.54107.6229
860.02180.08760.12430.55590.51630.7723-0.00180.0329-0.0631-0.22880.0213-0.05970.114-0.23230.21350.389-0.12990.030.435-0.22580.822822.3191.018399.8178
871.59110.77380.37530.49110.30030.2411-0.09390.29450.0461-0.0603-0.01830.06330.0089-0.29780.09520.4401-0.10130.03070.4719-0.1550.64267.43664.7208104.3908
880.75630.5045-0.54310.6116-0.74180.9986-0.1213-0.0077-0.07740.1107-0.0340.2216-0.057-0.31460.0890.41340.00120.05730.4117-0.04070.63567.061710.4385113.5523
891.0987-0.25980.30550.43380.04571.0635-0.0561-0.0050.0828-0.0417-0.02910.1271-0.019-0.1837-0.19150.32680.0050.15250.20820.04680.532827.09469.4826124.5375
900.0851-0.30430.02791.1107-0.15750.44650.0942-0.0468-0.07220.1642-0.05270.23110.0336-0.10950.04570.3351-0.03360.16850.22790.05580.785330.5434-0.2908122.4437
910.7524-0.00520.08230.3763-0.02430.1535-0.10130.03520.11070.09910.07180.0379-0.1257-0.0091-0.00510.36050.00240.01370.21470.01280.241254.237231.0211119.3469
921.50610.9585-0.08081.9814-0.13091.7518-0.04580.12630.0058-0.02220.104-0.2564-0.0940.2019-0.31260.2977-0.02740.02540.2838-0.02290.215978.890214.4931112.0746
930.2783-0.3865-0.01190.96660.07840.0663-0.1506-0.0311-0.19970.19870.09510.12120.08130.02090.04730.36260.0170.03430.25270.00460.26969.54798.2887121.6163
940.0781-0.0105-0.06530.1824-0.13220.2825-0.178-0.16280.16320.14360.16510.07660.09540.05510.17820.4020.0182-0.0080.2622-0.0010.237167.920125.8038126.9269
951.555-0.57280.30260.64270.21890.3356-0.1031-0.0425-0.04940.1402-0.01110.4409-0.0504-0.1266-0.00480.3937-0.01070.04990.26060.0060.478830.285931.4654119.025
961.5062-0.9232-0.55781.59150.44790.8116-0.01910.11390.20850.06150.18610.8755-0.1816-0.0461-0.16570.4605-0.05590.01860.30020.08160.528233.246761.7358116.6786
971.8929-0.2781-0.48990.2897-0.28750.65050.0943-0.1099-0.07620.7067-0.05450.0564-0.18040.1425-0.12040.6042-0.02150.08110.322-0.00280.418937.463152.0234127.1399
980.71570.37110.46920.91090.09370.54320.0045-0.09170.29410.01740.1125-0.6451-0.03110.02250.06060.3196-0.02210.05350.275-0.01260.595630.0012-23.9996116.8118
990.0720.0985-0.09870.0854-0.10970.15410.08280.10120.0633-0.24610.0226-1.11740.02630.4470.38830.0363-0.30340.34120.2348-0.04881.822656.8717-18.8534112.5413
1000.57610.5409-0.30480.8373-0.09140.48770.1488-0.0776-0.07870.2443-0.0202-0.2325-0.11990.14650.10570.3718-0.0608-0.02880.2992-0.13890.959840.9291-13.0625122.9615
1010.5317-0.1675-0.16190.46650.15410.19050.0144-0.0894-0.2268-0.05180.0153-0.13580.1853-0.0230.15850.3782-0.03090.00070.29580.04250.354717.619-44.2633119.1949
1021.1621-0.133-0.3650.48630.19430.62080.03250.0302-0.0347-0.0431-0.00060.24740.0638-0.2230.26650.3322-0.03720.00190.30810.02640.2895-6.7368-30.2176111.1434
1030.691-0.02190.13790.36020.09470.51850.0113-0.17040.01010.14880.0270.2195-0.0999-0.0984-0.32030.3371-0.01610.04090.31080.01230.28120.3045-24.3867120.0544
1040.56920.04670.53681.0580.31641.3839-0.0988-0.11870.21820.09860.1043-0.71670.07210.0459-0.27620.2033-0.0073-0.02460.1067-0.01250.742341.5846-44.6934119.7816
1050.31320.2272-0.03590.2802-0.03790.33360.0971-0.0170.0450.4408-0.0564-0.76670.2458-0.04260.24680.4174-0.1035-0.04580.223-0.02960.586136.2965-75.0576119.3888
1060.075-0.02850.06450.0115-0.01710.0531-0.11630.02020.1630.3859-0.1591-0.15220.2734-0.1902-0.31560.4064-0.0986-0.14540.2575-0.09540.674340.1264-57.1762129.3879
Refinement TLS group
IDRefine-IDRefine TLS-IDSelection detailsAuth asym-IDAuth seq-ID
1X-RAY DIFFRACTION1chain 'A' and (resid 2 through 69 )A2 - 69
2X-RAY DIFFRACTION2chain 'A' and (resid 70 through 130 )A70 - 130
3X-RAY DIFFRACTION3chain 'A' and (resid 131 through 179 )A131 - 179
4X-RAY DIFFRACTION4chain 'A' and (resid 180 through 248 )A180 - 248
5X-RAY DIFFRACTION5chain 'A' and (resid 249 through 268 )A249 - 268
6X-RAY DIFFRACTION6chain 'A' and (resid 269 through 288 )A269 - 288
7X-RAY DIFFRACTION7chain 'B' and (resid 2 through 95 )B2 - 95
8X-RAY DIFFRACTION8chain 'B' and (resid 96 through 216 )B96 - 216
9X-RAY DIFFRACTION9chain 'B' and (resid 217 through 288 )B217 - 288
10X-RAY DIFFRACTION10chain 'C' and (resid 2 through 95 )C2 - 95
11X-RAY DIFFRACTION11chain 'C' and (resid 96 through 216 )C96 - 216
12X-RAY DIFFRACTION12chain 'C' and (resid 217 through 268 )C217 - 268
13X-RAY DIFFRACTION13chain 'C' and (resid 269 through 288 )C269 - 288
14X-RAY DIFFRACTION14chain 'D' and (resid 2 through 41 )D2 - 41
15X-RAY DIFFRACTION15chain 'D' and (resid 42 through 95 )D42 - 95
16X-RAY DIFFRACTION16chain 'D' and (resid 96 through 153 )D96 - 153
17X-RAY DIFFRACTION17chain 'D' and (resid 154 through 179 )D154 - 179
18X-RAY DIFFRACTION18chain 'D' and (resid 180 through 248 )D180 - 248
19X-RAY DIFFRACTION19chain 'D' and (resid 249 through 268 )D249 - 268
20X-RAY DIFFRACTION20chain 'D' and (resid 269 through 288 )D269 - 288
21X-RAY DIFFRACTION21chain 'E' and (resid 2 through 41 )E2 - 41
22X-RAY DIFFRACTION22chain 'E' and (resid 42 through 95 )E42 - 95
23X-RAY DIFFRACTION23chain 'E' and (resid 96 through 130 )E96 - 130
24X-RAY DIFFRACTION24chain 'E' and (resid 131 through 153 )E131 - 153
25X-RAY DIFFRACTION25chain 'E' and (resid 154 through 179 )E154 - 179
26X-RAY DIFFRACTION26chain 'E' and (resid 180 through 195 )E180 - 195
27X-RAY DIFFRACTION27chain 'E' and (resid 196 through 216 )E196 - 216
28X-RAY DIFFRACTION28chain 'E' and (resid 217 through 248 )E217 - 248
29X-RAY DIFFRACTION29chain 'E' and (resid 249 through 268 )E249 - 268
30X-RAY DIFFRACTION30chain 'E' and (resid 269 through 288 )E269 - 288
31X-RAY DIFFRACTION31chain 'F' and (resid 2 through 95 )F2 - 95
32X-RAY DIFFRACTION32chain 'F' and (resid 96 through 288 )F96 - 288
33X-RAY DIFFRACTION33chain 'G' and (resid 2 through 41 )G2 - 41
34X-RAY DIFFRACTION34chain 'G' and (resid 42 through 95 )G42 - 95
35X-RAY DIFFRACTION35chain 'G' and (resid 96 through 216 )G96 - 216
36X-RAY DIFFRACTION36chain 'G' and (resid 217 through 248 )G217 - 248
37X-RAY DIFFRACTION37chain 'G' and (resid 249 through 268 )G249 - 268
38X-RAY DIFFRACTION38chain 'G' and (resid 269 through 288 )G269 - 288
39X-RAY DIFFRACTION39chain 'H' and (resid 2 through 95 )H2 - 95
40X-RAY DIFFRACTION40chain 'H' and (resid 96 through 288 )H96 - 288
41X-RAY DIFFRACTION41chain 'I' and (resid 2 through 95 )I2 - 95
42X-RAY DIFFRACTION42chain 'I' and (resid 96 through 216 )I96 - 216
43X-RAY DIFFRACTION43chain 'I' and (resid 217 through 268 )I217 - 268
44X-RAY DIFFRACTION44chain 'I' and (resid 269 through 288 )I269 - 288
45X-RAY DIFFRACTION45chain 'J' and (resid 2 through 113 )J2 - 113
46X-RAY DIFFRACTION46chain 'J' and (resid 114 through 130 )J114 - 130
47X-RAY DIFFRACTION47chain 'J' and (resid 131 through 179 )J131 - 179
48X-RAY DIFFRACTION48chain 'J' and (resid 180 through 248 )J180 - 248
49X-RAY DIFFRACTION49chain 'J' and (resid 249 through 268 )J249 - 268
50X-RAY DIFFRACTION50chain 'J' and (resid 269 through 288 )J269 - 288
51X-RAY DIFFRACTION51chain 'K' and (resid 2 through 95 )K2 - 95
52X-RAY DIFFRACTION52chain 'K' and (resid 96 through 248 )K96 - 248
53X-RAY DIFFRACTION53chain 'K' and (resid 249 through 288 )K249 - 288
54X-RAY DIFFRACTION54chain 'L' and (resid 2 through 95 )L2 - 95
55X-RAY DIFFRACTION55chain 'L' and (resid 96 through 216 )L96 - 216
56X-RAY DIFFRACTION56chain 'L' and (resid 217 through 288 )L217 - 288
57X-RAY DIFFRACTION57chain 'M' and (resid 2 through 113 )M2 - 113
58X-RAY DIFFRACTION58chain 'M' and (resid 114 through 288 )M114 - 288
59X-RAY DIFFRACTION59chain 'N' and (resid 2 through 95 )N2 - 95
60X-RAY DIFFRACTION60chain 'N' and (resid 96 through 216 )N96 - 216
61X-RAY DIFFRACTION61chain 'N' and (resid 217 through 288 )N217 - 288
62X-RAY DIFFRACTION62chain 'O' and (resid 2 through 41 )O2 - 41
63X-RAY DIFFRACTION63chain 'O' and (resid 42 through 95 )O42 - 95
64X-RAY DIFFRACTION64chain 'O' and (resid 96 through 153 )O96 - 153
65X-RAY DIFFRACTION65chain 'O' and (resid 154 through 248 )O154 - 248
66X-RAY DIFFRACTION66chain 'O' and (resid 249 through 288 )O249 - 288
67X-RAY DIFFRACTION67chain 'P' and (resid 2 through 41 )P2 - 41
68X-RAY DIFFRACTION68chain 'P' and (resid 42 through 113 )P42 - 113
69X-RAY DIFFRACTION69chain 'P' and (resid 114 through 130 )P114 - 130
70X-RAY DIFFRACTION70chain 'P' and (resid 131 through 153 )P131 - 153
71X-RAY DIFFRACTION71chain 'P' and (resid 154 through 179 )P154 - 179
72X-RAY DIFFRACTION72chain 'P' and (resid 180 through 195 )P180 - 195
73X-RAY DIFFRACTION73chain 'P' and (resid 196 through 216 )P196 - 216
74X-RAY DIFFRACTION74chain 'P' and (resid 217 through 248 )P217 - 248
75X-RAY DIFFRACTION75chain 'P' and (resid 249 through 268 )P249 - 268
76X-RAY DIFFRACTION76chain 'P' and (resid 269 through 288 )P269 - 288
77X-RAY DIFFRACTION77chain 'Q' and (resid 2 through 95 )Q2 - 95
78X-RAY DIFFRACTION78chain 'Q' and (resid 96 through 195 )Q96 - 195
79X-RAY DIFFRACTION79chain 'Q' and (resid 196 through 288 )Q196 - 288
80X-RAY DIFFRACTION80chain 'R' and (resid 2 through 95 )R2 - 95
81X-RAY DIFFRACTION81chain 'R' and (resid 96 through 216 )R96 - 216
82X-RAY DIFFRACTION82chain 'R' and (resid 217 through 288 )R217 - 288
83X-RAY DIFFRACTION83chain 'S' and (resid 2 through 95 )S2 - 95
84X-RAY DIFFRACTION84chain 'S' and (resid 96 through 113 )S96 - 113
85X-RAY DIFFRACTION85chain 'S' and (resid 114 through 153 )S114 - 153
86X-RAY DIFFRACTION86chain 'S' and (resid 154 through 179 )S154 - 179
87X-RAY DIFFRACTION87chain 'S' and (resid 180 through 195 )S180 - 195
88X-RAY DIFFRACTION88chain 'S' and (resid 196 through 248 )S196 - 248
89X-RAY DIFFRACTION89chain 'S' and (resid 249 through 268 )S249 - 268
90X-RAY DIFFRACTION90chain 'S' and (resid 269 through 288 )S269 - 288
91X-RAY DIFFRACTION91chain 'T' and (resid 2 through 95 )T2 - 95
92X-RAY DIFFRACTION92chain 'T' and (resid 96 through 216 )T96 - 216
93X-RAY DIFFRACTION93chain 'T' and (resid 217 through 268 )T217 - 268
94X-RAY DIFFRACTION94chain 'T' and (resid 269 through 288 )T269 - 288
95X-RAY DIFFRACTION95chain 'U' and (resid 2 through 95 )U2 - 95
96X-RAY DIFFRACTION96chain 'U' and (resid 96 through 216 )U96 - 216
97X-RAY DIFFRACTION97chain 'U' and (resid 217 through 288 )U217 - 288
98X-RAY DIFFRACTION98chain 'V' and (resid 2 through 95 )V2 - 95
99X-RAY DIFFRACTION99chain 'V' and (resid 96 through 268 )V96 - 268
100X-RAY DIFFRACTION100chain 'V' and (resid 269 through 288 )V269 - 288
101X-RAY DIFFRACTION101chain 'W' and (resid 2 through 95 )W2 - 95
102X-RAY DIFFRACTION102chain 'W' and (resid 96 through 195 )W96 - 195
103X-RAY DIFFRACTION103chain 'W' and (resid 196 through 288 )W196 - 288
104X-RAY DIFFRACTION104chain 'X' and (resid 2 through 95 )X2 - 95
105X-RAY DIFFRACTION105chain 'X' and (resid 96 through 248 )X96 - 248
106X-RAY DIFFRACTION106chain 'X' and (resid 249 through 288 )X249 - 288

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