解像度: 2.3→45.94 Å / Cor.coef. Fo:Fc: 0.907 / Cor.coef. Fo:Fc free: 0.885 / SU R Cruickshank DPI: 0.31 / 交差検証法: THROUGHOUT / σ(F): 0 / SU R Blow DPI: 0.39 / SU Rfree Blow DPI: 0.26 / SU Rfree Cruickshank DPI: 0.239 詳細: Even if collection were carried out at 2.2 angstrom resoltuion, the anisotropic nature of the data had a harmfull impact on model refinement especially when the 2.2 - 2.3 shell was included. ...詳細: Even if collection were carried out at 2.2 angstrom resoltuion, the anisotropic nature of the data had a harmfull impact on model refinement especially when the 2.2 - 2.3 shell was included. Refinement was carried out at 2.3 angstrom as maximum resolution.