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Open data
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Basic information
Entry | Database: PDB / ID: 6hnb | ||||||
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Title | Crystal structure of aminotransferase Aro8 from Candida albicans | ||||||
![]() | Aromatic amino acid aminotransferase I | ||||||
![]() | TRANSFERASE / CaAro8 | ||||||
Function / homology | ![]() transaminase activity / biosynthetic process / pyridoxal phosphate binding Similarity search - Function | ||||||
Biological species | ![]() | ||||||
Method | ![]() ![]() ![]() | ||||||
![]() | Kiliszek, A. / Rzad, K. / Rypniewski, W. / Milewski, S. / Gabriel, I. | ||||||
Funding support | ![]()
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![]() | ![]() Title: Crystal structures of aminotransferases Aro8 and Aro9 from Candida albicans and structural insights into their properties. Authors: Kiliszek, A. / Rypniewski, W. / Rzad, K. / Milewski, S. / Gabriel, I. | ||||||
History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 222.1 KB | Display | ![]() |
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PDB format | ![]() | 175.7 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Summary document | ![]() | 463.7 KB | Display | ![]() |
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Full document | ![]() | 468.6 KB | Display | |
Data in XML | ![]() | 44.4 KB | Display | |
Data in CIF | ![]() | 67.8 KB | Display | |
Arichive directory | ![]() ![]() | HTTPS FTP |
-Related structure data
Related structure data | ![]() 6hndC ![]() 6hnuC ![]() 6hnvC ![]() 4je5S S: Starting model for refinement C: citing same article ( |
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Similar structure data |
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Links
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Assembly
Deposited unit | ![]()
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Unit cell |
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Components
#1: Protein | Mass: 54870.160 Da / Num. of mol.: 2 Source method: isolated from a genetically manipulated source Source: (gene. exp.) ![]() Production host: ![]() ![]() References: UniProt: C4YJ02 #2: Chemical | #3: Chemical | #4: Chemical | ChemComp-CL / #5: Water | ChemComp-HOH / | |
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-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 2.41 Å3/Da / Density % sol: 48.98 % |
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Crystal grow | Temperature: 292 K / Method: vapor diffusion, sitting drop / Details: 0.2 M MgCl2, 0.1 M Bis-Tris pH 5.5, 25% PEG 3350 |
-Data collection
Diffraction | Mean temperature: 100 K |
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Diffraction source | Source: ![]() ![]() ![]() |
Detector | Type: MARMOSAIC 225 mm CCD / Detector: CCD / Date: Aug 26, 2016 |
Radiation | Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Wavelength: 0.895 Å / Relative weight: 1 |
Reflection | Resolution: 1.96→50 Å / Num. obs: 76434 / % possible obs: 99.4 % / Redundancy: 7.1 % / CC1/2: 0.997 / Rmerge(I) obs: 0.148 / Net I/σ(I): 13.05 |
Reflection shell | Resolution: 1.96→2.08 Å / Redundancy: 7 % / Mean I/σ(I) obs: 2.03 / Num. unique obs: 11840 / CC1/2: 0.697 / % possible all: 96.6 |
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Processing
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Refinement | Method to determine structure: ![]() Starting model: 4JE5 Resolution: 1.96→48.29 Å / Cor.coef. Fo:Fc: 0.957 / Cor.coef. Fo:Fc free: 0.924 / SU B: 4.509 / SU ML: 0.122 / Cross valid method: THROUGHOUT / ESU R: 0.163 / ESU R Free: 0.157 / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
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Solvent computation | Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Displacement parameters | Biso mean: 24.991 Å2
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Refinement step | Cycle: 1 / Resolution: 1.96→48.29 Å
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Refine LS restraints |
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