- PDB-6e7e: High resolution crystal structure of IncA soluble domain -
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Open data
ID or keywords:
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Basic information
Entry
Database: PDB / ID: 6e7e
Title
High resolution crystal structure of IncA soluble domain
Components
Inclusion membrane protein A
Keywords
PROTEIN BINDING / membrane fusion / chlamydia / SNARE-like protein / inclusion
Function / homology
pathogen-containing vacuole membrane / host cell membrane / extracellular region / membrane / Inclusion membrane protein A / Inclusion membrane protein A
Function and homology information
Biological species
Chlamydia trachomatis (bacteria)
Method
X-RAY DIFFRACTION / SYNCHROTRON / SAD / Resolution: 1.12 Å
Monochromator: double crystal Si(111) / Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 0.98 Å / Relative weight: 1
Reflection
Resolution: 1.12→15 Å / Num. obs: 52606 / % possible obs: 91.3 % / Redundancy: 7.3 % / Biso Wilson estimate: 10.8 Å2 / Rsym value: 0.055 / Net I/σ(I): 47.9
Reflection shell
Resolution: 1.12→1.16 Å / Mean I/σ(I) obs: 4.7 / Num. unique obs: 2307 / Rsym value: 0.298 / % possible all: 55
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Processing
Software
Name
Version
Classification
REFMAC
5.8.0241
refinement
PDB_EXTRACT
3.24
dataextraction
HKL-2000
datareduction
HKL-2000
datascaling
AutoSol
phasing
Refinement
Method to determine structure: SAD / Resolution: 1.12→14.96 Å / Cor.coef. Fo:Fc: 0.977 / Cor.coef. Fo:Fc free: 0.965 / SU B: 1.021 / SU ML: 0.022 / Cross valid method: THROUGHOUT / ESU R: 0.034 / ESU R Free: 0.035 / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.169
2010
3.8 %
RANDOM
Rwork
0.141
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obs
0.142
50533
90.7 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.1 Å