Details | Type | Solution-ID | Contents | Details | Label | Solvent system |
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solution1 | 1 mM TP3-T6, 70 mM potassium chloride, 7.7 mM KH2PO4, 12.3 mM K2HPO4, 90% H2O/10% D2O | 1mM TP3-T6 oligonucleotide sample in H2O solvent | TP3-T6-H2O | 90% H2O/10% D2Osolution2 | 1 mM TP3-T6, 70 mM potassium chloride, 7.7 mM KH2PO4, 12.3 mM K2HPO4, 100% D2O | 1mM TP3-T6 oligonucleotide sample in D2O solvent | TP3-T6-D2O | 100% D2Osolution3 | 0.4 mM U-4% 15N Guanine TP3-T6, 70 mM potassium chloride, 7.7 mM KH2PO4, 12.3 mM K2HPO4, 90% H2O/10% D2O | 0.4 mM 4%-15N labeled TP3-T6 oligonucleotides samples in H2O solvent | 15N_samples90% H2O/10% D2O | | | | | | |
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Sample | Conc. (mg/ml) | Component | Isotopic labeling | Solution-ID |
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1 mMTP3-T6 | natural abundance1 | 70 mMpotassium chloridenatural abundance1 | 7.7 mMKH2PO4natural abundance1 | 12.3 mMK2HPO4natural abundance1 | 1 mMTP3-T6 | natural abundance2 | 70 mMpotassium chloridenatural abundance2 | 7.7 mMKH2PO4natural abundance2 | 12.3 mMK2HPO4natural abundance2 | 0.4 mMTP3-T6 | U-4% 15N Guanine | 3 | 70 mMpotassium chloridenatural abundance3 | 7.7 mMKH2PO4natural abundance3 | 12.3 mMK2HPO4natural abundance3 | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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Sample conditions | Conditions-ID | Details | Ionic strength | Label | pH | Pressure (kPa) | Temperature (K) |
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1 | 70 mM KCl, 20 mM KPi, pH 7.0100 mMPhosphate buffer7 1 atm298 K2 | 70 mM KCl, 20 mM KPi, pH 7.0100 mMLow temperature phosphate buffer7 1 atm283 K | | | | | | | | | | | |
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