Monochromator: double crystal / Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray
Radiation wavelength
Wavelength: 0.979 Å / Relative weight: 1
Reflection
Resolution: 2.3→50 Å
-
Phasing
Phasing
Method: molecular replacement
Phasing MR
Model details: Phaser MODE: MR_AUTO
Highest resolution
Lowest resolution
Rotation
2.3 Å
33.45 Å
Translation
2.3 Å
33.45 Å
-
Processing
Software
Name
Version
Classification
NB
SCALEPACK
datascaling
PHASER
2.5.1
phasing
REFMAC
refinement
PDB_EXTRACT
3.11
dataextraction
DENZO
datareduction
Refinement
Resolution: 2.3→33.48 Å / Cor.coef. Fo:Fc: 0.939 / Cor.coef. Fo:Fc free: 0.912 / SU B: 5.671 / SU ML: 0.139 / Cross valid method: THROUGHOUT / ESU R: 0.243 / ESU R Free: 0.209 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.2517
1207
5.1 %
RANDOM
Rwork
0.20706
-
-
-
obs
0.20936
22425
98.45 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK