温度: 297 K / 手法: 蒸気拡散法, ハンギングドロップ法 / pH: 4.6 詳細: 20 mg/mL protein (in 10 mM BTP pH 7.5) mixed 1:1 with reservoir liquor containing 100 mM NaOAc (pH 4.6) and 0.6-3.0 M NaCl, cryoprotectant solution, comprising 20% glycerol and reservoir ...詳細: 20 mg/mL protein (in 10 mM BTP pH 7.5) mixed 1:1 with reservoir liquor containing 100 mM NaOAc (pH 4.6) and 0.6-3.0 M NaCl, cryoprotectant solution, comprising 20% glycerol and reservoir solution, Vapor diffusion, hanging drop, temperature 297K, VAPOR DIFFUSION, HANGING DROP
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データ収集
回折
平均測定温度: 120 K
放射光源
由来: 回転陽極 / タイプ: RIGAKU MICROMAX-007 / 波長: 1.5418 Å
解像度: 2.1→37.09 Å / Cor.coef. Fo:Fc: 0.951 / Cor.coef. Fo:Fc free: 0.937 / WRfactor Rfree: 0.247 / WRfactor Rwork: 0.2124 / Occupancy max: 1 / Occupancy min: 0.35 / FOM work R set: 0.8057 / SU B: 11.955 / SU ML: 0.148 / SU R Cruickshank DPI: 0.2548 / SU Rfree: 0.2005 / 交差検証法: THROUGHOUT / σ(F): 0 / ESU R: 0.255 / ESU R Free: 0.2 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: U VALUES WITH TLS ADDED HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.2499
3143
5 %
RANDOM
Rwork
0.217
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obs
0.2186
62592
91.78 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK