ソフトウェア | 名称 | バージョン | 分類 | NB |
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DENZO | | データ削減 | | SCALEPACK | | データスケーリング | | REFMAC | 5.6.0117精密化 | | PDB_EXTRACT | 3.11 | データ抽出 | | Blu-Ice | | データ収集 | | BALBES | | 位相決定 | | |
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精密化 | 構造決定の手法: 分子置換 開始モデル: PDB ENTRY 2QCB 解像度: 1.5→36.94 Å / Cor.coef. Fo:Fc: 0.947 / Cor.coef. Fo:Fc free: 0.935 / Occupancy max: 1 / Occupancy min: 0.45 / SU B: 2.483 / SU ML: 0.05 / 交差検証法: THROUGHOUT / σ(F): 0 / ESU R: 0.095 / ESU R Free: 0.094 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS U VALUES : WITH TLS ADDED
| Rfactor | 反射数 | %反射 | Selection details |
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Rfree | 0.2299 | 3343 | 5 % | RANDOM |
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Rwork | 0.2006 | - | - | - |
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obs | 0.2021 | 63726 | 100 % | - |
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all | - | 63726 | - | - |
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溶媒の処理 | イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK |
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原子変位パラメータ | Biso max: 93.85 Å2 / Biso mean: 25.9489 Å2 / Biso min: 13.2 Å2
| Baniso -1 | Baniso -2 | Baniso -3 |
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1- | -0.02 Å2 | 0 Å2 | 0 Å2 |
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2- | - | 0.14 Å2 | 0 Å2 |
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3- | - | - | -0.12 Å2 |
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精密化ステップ | サイクル: LAST / 解像度: 1.5→36.94 Å
| タンパク質 | 核酸 | リガンド | 溶媒 | 全体 |
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原子数 | 3683 | 0 | 70 | 366 | 4119 |
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拘束条件 | Refine-ID | タイプ | Dev ideal | Dev ideal target | 数 |
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X-RAY DIFFRACTION | r_bond_refined_d0.013 | 0.02 | 3878 | X-RAY DIFFRACTION | r_bond_other_d0.001 | 0.02 | 2405 | X-RAY DIFFRACTION | r_angle_refined_deg1.671 | 1.912 | 5300 | X-RAY DIFFRACTION | r_angle_other_deg1.983 | 3 | 5845 | X-RAY DIFFRACTION | r_dihedral_angle_1_deg6.823 | 5 | 489 | X-RAY DIFFRACTION | r_dihedral_angle_2_deg29.756 | 23.58 | 162 | X-RAY DIFFRACTION | r_dihedral_angle_3_deg13.018 | 15 | 520 | X-RAY DIFFRACTION | r_dihedral_angle_4_deg17.95 | 15 | 20 | X-RAY DIFFRACTION | r_chiral_restr0.124 | 0.2 | 591 | X-RAY DIFFRACTION | r_gen_planes_refined0.008 | 0.02 | 4448 | X-RAY DIFFRACTION | r_gen_planes_other0.001 | 0.02 | 876 | | | | | | | | | | | |
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LS精密化 シェル | 解像度: 1.5→1.539 Å / Total num. of bins used: 20
| Rfactor | 反射数 | %反射 |
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Rfree | 0.229 | 183 | - |
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Rwork | 0.207 | 3698 | - |
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all | - | 3881 | - |
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obs | - | - | 72.04 % |
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精密化 TLS | 手法: refined / Refine-ID: X-RAY DIFFRACTION ID | L11 (°2) | L12 (°2) | L13 (°2) | L22 (°2) | L23 (°2) | L33 (°2) | S11 (Å °) | S12 (Å °) | S13 (Å °) | S21 (Å °) | S22 (Å °) | S23 (Å °) | S31 (Å °) | S32 (Å °) | S33 (Å °) | T11 (Å2) | T12 (Å2) | T13 (Å2) | T22 (Å2) | T23 (Å2) | T33 (Å2) | Origin x (Å) | Origin y (Å) | Origin z (Å) |
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1 | 8.4516 | -1.7792 | 1.3053 | 0.646 | 1.2686 | 9.0604 | 0.0476 | -0.2363 | 0.2321 | -0.0671 | 0.0797 | -0.0937 | -0.4008 | 0.1875 | -0.1273 | 0.1413 | -0.0296 | -0.0541 | 0.1856 | -0.006 | 0.1814 | 42.9706 | -1.9729 | 34.1844 | 2 | 4.3452 | 1.6095 | -0.3885 | 3.1667 | -0.5482 | 0.9963 | -0.0749 | -0.0329 | -0.1107 | 0.0206 | 0.0419 | -0.1706 | -0.0192 | -0.0156 | 0.033 | 0.0798 | -0.0008 | -0.0064 | 0.1299 | -0.0276 | 0.1016 | 40.7862 | -6.7064 | 31.0137 | 3 | 5.2509 | 3.2928 | -2.4287 | 7.5561 | -4.5151 | 3.9533 | -0.0079 | -0.2097 | -0.2826 | 0.1608 | -0.0619 | -0.1046 | 0.0707 | 0.0579 | 0.0697 | 0.0459 | 0.0121 | 0.0025 | 0.1143 | -0.0338 | 0.0908 | 41.3087 | -11.3296 | 28.1682 | 4 | 17.6898 | -0.9526 | -6.2402 | 27.2127 | -8.1675 | 6.3276 | -0.1144 | -1.305 | -0.2224 | 1.7225 | -0.1497 | -0.5525 | 0.395 | 0.6288 | 0.2642 | 0.6488 | 0.0516 | -0.033 | 0.179 | 0.0027 | 0.1167 | 44.8635 | -20.0898 | 30.5966 | 5 | 0.5788 | 0.1326 | 0.0973 | 3.3411 | -0.206 | 0.5275 | 0.0444 | -0.0358 | 0.0406 | 0.0842 | -0.0779 | -0.0728 | -0.0176 | 0.0273 | 0.0335 | 0.0234 | -0.0073 | -0.0042 | 0.1256 | -0.0059 | 0.1282 | 41.6851 | -4.0358 | 23.7981 | 6 | 8.5929 | -2.9117 | 3.4799 | 9.878 | 4.6 | 5.1662 | 0.0724 | -0.3085 | -0.6707 | 0.2826 | 0.2274 | 0.2088 | 0.2327 | -0.034 | -0.2998 | 0.035 | -0.0178 | 0.0118 | 0.1611 | 0.0255 | 0.1951 | 39.1882 | -24.0535 | 20.856 | 7 | 1.3903 | 0.5707 | 0.9179 | 7.4916 | 1.4271 | 0.9466 | -0.0348 | -0.0688 | 0.0875 | 0.0455 | -0.0214 | 0.1187 | -0.0399 | -0.0172 | 0.0562 | 0.0085 | -0.0178 | 0.0125 | 0.1143 | -0.0073 | 0.1219 | 35.5284 | -3.8977 | 24.6265 | 8 | 10.1434 | -4.5762 | 2.7281 | 11.9431 | 16.0951 | 31.579 | -0.0918 | -0.6613 | 0.0293 | 0.3891 | -0.0925 | 0.1331 | 0.1301 | -0.8546 | 0.1843 | 0.4561 | -0.0209 | 0.0511 | 0.2024 | -0.0532 | 0.1531 | 34.097 | 3.6452 | 37.5322 | 9 | 0.7939 | 0.4682 | 0.3036 | 1.3622 | 1.0013 | 3.8689 | -0.0123 | 0.024 | -0.0785 | 0.015 | 0.0104 | 0.0786 | -0.0095 | -0.0262 | 0.0019 | 0.0068 | 0.0019 | -0.0005 | 0.1203 | -0.0069 | 0.1314 | 31.2759 | -10.8774 | 20.6671 | 10 | 19.3996 | -10.0561 | -6.6334 | 12.0195 | 4.7196 | 6.9532 | 0.201 | 0.9422 | -0.3469 | -0.5199 | -0.2977 | 0.0274 | 0.0325 | -0.2594 | 0.0967 | 0.0956 | -0.0065 | -0.0207 | 0.2065 | -0.0284 | 0.1553 | 24.857 | -20.6903 | 8.0748 | 11 | 1.46 | 0.8246 | 2.0333 | 6.5276 | 5.9773 | 9.5453 | 0.0315 | -0.0038 | -0.0694 | 0.037 | -0.0887 | 0.203 | 0.0669 | -0.136 | 0.0572 | 0.0024 | -0.0066 | 0.0117 | 0.115 | -0.0029 | 0.1343 | 26.6323 | -13.129 | 20.2922 | 12 | 17.6266 | 3.7298 | 7.1574 | 8.0549 | 4.9318 | 13.6284 | -0.2293 | -0.9446 | 0.0124 | 0.44 | 0.0496 | -0.1319 | -0.0002 | 0.1212 | 0.1797 | 0.1135 | 0.0161 | 0.0064 | 0.1435 | -0.0073 | 0.1418 | 36.8566 | -4.1189 | 36.0235 | 13 | 4.4673 | -1.4039 | 0.3711 | 1.2345 | -0.1916 | 1.8014 | 0.0668 | 0.128 | -0.0296 | -0.1276 | 0.0207 | -0.0537 | -0.02 | 0.0512 | -0.0875 | 0.0695 | -0.0125 | 0.0126 | 0.1414 | -0.0218 | 0.1299 | 42.6566 | -7.565 | 4.2404 | 14 | 2.6298 | 4.2062 | -3.8457 | 13.7055 | -3.3177 | 6.7771 | -0.1211 | -0.2632 | -0.1931 | -0.0102 | -0.2008 | -0.2938 | 0.2887 | 0.4754 | 0.3219 | 0.0245 | 0.0223 | 0.0194 | 0.1611 | -0.0108 | 0.1664 | 48.334 | -9.5228 | 13.0394 | 15 | 19.0582 | -2.4637 | 4.1076 | 11.8745 | -4.3614 | 6.0132 | -0.2321 | 0.353 | 1.1164 | 0.1164 | 0.1478 | -0.0681 | -0.5228 | -0.1472 | 0.0843 | 0.1824 | -0.0079 | 0.0064 | 0.1148 | -0.0098 | 0.1446 | 38.259 | 4.1332 | 6.2989 | 16 | 14.6686 | 1.5723 | 1.797 | 18.4486 | -2.0706 | 18.732 | 0.2471 | 1.0128 | 0.8995 | -1.7776 | -0.1205 | -0.3182 | -0.804 | 0.3779 | -0.1266 | 0.2489 | 0.0082 | 0.057 | 0.2179 | 0.0349 | 0.2036 | 45.3827 | 7.8345 | 6.7951 | 17 | 1.111 | -0.4072 | -0.1964 | 2.2866 | -0.218 | 0.8603 | 0.0582 | 0.0683 | -0.1056 | -0.149 | -0.0722 | -0.0997 | 0.1521 | 0.0183 | 0.014 | 0.0477 | 0.0064 | 0.0046 | 0.1304 | -0.015 | 0.1226 | 41.0445 | -12.5351 | 13.0865 | 18 | 9.3427 | 1.0313 | -4.9296 | 20.1527 | -6.3497 | 13.6797 | 0.0285 | 0.1784 | 0.1053 | -0.3194 | -0.091 | -0.1337 | -0.4391 | 0.2978 | 0.0625 | 0.039 | -0.021 | 0.011 | 0.1441 | -0.0248 | 0.1608 | 45.4082 | 11.6034 | 13.3781 | 19 | 0.6998 | 0.0066 | -0.2728 | 1.9603 | 0.6292 | 0.8398 | -0.05 | 0.0486 | -0.0073 | -0.059 | 0.0112 | 0.1517 | 0.0305 | 0.0161 | 0.0387 | 0.0148 | 0.0065 | -0.0033 | 0.118 | -0.0099 | 0.12 | 36.9692 | -5.5063 | 11.4492 | 20 | 7.9301 | -6.951 | -13.2721 | 6.3327 | 11.7426 | 22.2641 | 0.0714 | 0.8295 | -0.2166 | -0.2888 | -0.478 | 0.2362 | -0.1705 | -1.2831 | 0.4066 | 0.3654 | -0.162 | -0.0657 | 0.3245 | 0.0039 | 0.1279 | 34.9798 | -13.1429 | 1.0226 | 21 | 1.1923 | -0.1336 | 0.126 | 2.8338 | 3.0719 | 5.7824 | -0.0156 | -0.0407 | 0.1387 | 0.0811 | 0.0182 | 0.0429 | 0.0091 | -0.0369 | -0.0026 | 0.0201 | -0.0011 | 0.0052 | 0.1058 | -0.001 | 0.1355 | 30.8457 | 0.6801 | 17.4418 | 22 | 17.4158 | 7.9344 | 2.9586 | 13.1029 | 4.8002 | 6.8705 | 0.0222 | -0.7798 | 0.3671 | 0.4078 | -0.2007 | 0.1254 | 0.0147 | -0.195 | 0.1784 | 0.0577 | 0.0029 | 0.0231 | 0.1809 | -0.0492 | 0.1726 | 24.2501 | 8.1704 | 27.4803 | 23 | 3.8201 | -1.671 | -2.7515 | 1.0873 | 1.6851 | 3.9704 | 0.1413 | 0.2105 | 0.1027 | -0.1808 | -0.0613 | -0.0289 | -0.149 | -0.0903 | -0.08 | 0.062 | -0.0078 | 0.0077 | 0.0873 | 0.0072 | 0.1359 | 34.3358 | -3.8552 | 7.2498 | 24 | 2.9066 | -2.9014 | -3.1762 | 11.5385 | 8.6978 | 7.0065 | 0.0503 | -0.2556 | -0.1695 | 0.3578 | 0.0257 | -0.2751 | 0.2184 | 0.1284 | -0.076 | 0.1414 | -0.0218 | 0.0125 | 0.2528 | 0.0074 | 0.2267 | 45.0225 | -17.5995 | -1.9176 | 25 | 5.8189 | -1.495 | 0.2242 | 0.4152 | -0.4698 | 5.5518 | 0.0024 | -0.0971 | -0.3408 | -0.013 | 0.0423 | 0.0922 | 0.3031 | -0.0448 | -0.0447 | 0.1301 | 0.0155 | 0.0267 | 0.1842 | 0.009 | 0.1821 | 4.1436 | -9.3601 | 32.4526 | 26 | 9.7618 | -2.6591 | 1.5012 | 2.163 | -2.4436 | 7.6051 | 0.0043 | -0.4865 | 0.3846 | 0.4223 | 0.0391 | -0.0274 | -0.4806 | -0.1975 | -0.0434 | 0.1972 | 0 | 0.0328 | 0.1587 | -0.0512 | 0.1602 | 14.1709 | 2.445 | 32.8901 | 27 | 6.4129 | 6.4584 | 0.5436 | 14.1122 | 2.2176 | 2.155 | -0.1085 | -0.1077 | 0.0815 | -0.3166 | 0.0061 | 0.1426 | -0.1883 | -0.2229 | 0.1024 | 0.1107 | 0.0236 | 0.0153 | 0.1771 | 0.0165 | 0.1293 | 2.4172 | -6.3657 | 27.3941 | 28 | 3.8006 | -1.3535 | 0.3555 | 1.9931 | 1.7537 | 2.6001 | -0.1367 | -0.0165 | 0.4711 | -0.1223 | -0.0505 | 0.1036 | -0.4069 | -0.0679 | 0.1872 | 0.1733 | 0.008 | 0.1064 | 0.163 | -0.0102 | 0.2653 | 6.5274 | 1.7899 | 25.4887 | 29 | 1.0697 | -0.5298 | 0.1972 | 1.8139 | -0.3848 | 0.3784 | -0.02 | -0.0844 | 0.0044 | 0.2166 | 0.0448 | 0.1633 | -0.0615 | -0.0492 | -0.0248 | 0.0602 | 0.0054 | 0.0173 | 0.1288 | -0.0062 | 0.1316 | 7.2972 | -6.8508 | 23.9616 | 30 | 7.9543 | -4.3576 | -3.1537 | 17.091 | 2.2232 | 4.4375 | 0.0571 | -0.0558 | 0.3614 | -0.3715 | -0.0751 | -0.1233 | -0.1926 | -0.1898 | 0.018 | 0.0469 | 0.0176 | -0.0019 | 0.1275 | -0.006 | 0.2094 | 4.1951 | 12.0135 | 17.774 | 31 | 1.3166 | -0.2869 | 0.146 | 5.3006 | -2.7984 | 2.4478 | -0.036 | -0.0765 | 0.0544 | 0.1911 | -0.0116 | -0.0638 | -0.1001 | -0.0218 | 0.0476 | 0.0317 | -0.0063 | 0.0043 | 0.1099 | -0.0193 | 0.1177 | 12.5386 | -3.6962 | 22.8784 | 32 | 7.6588 | -0.9134 | -1.0925 | 11.1481 | -10.3395 | 32.0524 | -0.2597 | -1.0031 | 0.0556 | 1.0879 | -0.2942 | -0.3881 | 0.4946 | 0.5062 | 0.5539 | 0.2887 | -0.0283 | 0.0068 | 0.2472 | 0.0148 | 0.1475 | 13.6102 | -9.6353 | 37.5992 | 33 | 1.303 | 0.8066 | -0.9743 | 3.9249 | -4.3268 | 8.7062 | -0.0035 | 0.0309 | 0.1434 | -0.0982 | 0.0366 | -0.0081 | 0.1565 | -0.0536 | -0.0331 | 0.0115 | -0.0024 | -0.0017 | 0.1045 | -0.0075 | 0.1397 | 18.3966 | -0.3558 | 17.736 | 34 | 24.9863 | -12.2879 | 6.755 | 7.1836 | -8.1995 | 22.7617 | 0.2453 | 0.9497 | 0.2085 | -0.2771 | -0.4789 | -0.1301 | 0.6275 | 0.3731 | 0.2337 | 0.2294 | -0.0535 | -0.0104 | 0.1793 | 0.0515 | 0.1467 | 25.2075 | 5.5598 | 5.0286 | 35 | 2.9507 | 1.5532 | -3.8697 | 2.8948 | -4.0721 | 12.259 | -0.0085 | -0.0205 | 0.0695 | 0.1267 | -0.042 | -0.0914 | -0.0979 | 0.0379 | 0.0505 | 0.0214 | -0.0017 | -0.0043 | 0.0895 | -0.0162 | 0.1451 | 22.052 | 0.6107 | 19.7362 | 36 | 2.6174 | -2.4276 | -0.3162 | 2.6025 | 0.412 | 8.5111 | -0.079 | -0.5503 | -0.1467 | 0.3206 | 0.299 | 0.3997 | -0.3613 | -0.1679 | -0.22 | 0.2997 | -0.0719 | 0.1324 | 0.3026 | -0.1378 | 0.2925 | 7.4869 | -5.0094 | 36.5353 | 37 | 10.237 | 1.515 | -0.7552 | 0.2748 | 0.4544 | 6.4632 | 0.0555 | 0.1436 | 0.3262 | -0.033 | 0.0113 | 0.0526 | -0.4013 | -0.1078 | -0.0669 | 0.1331 | -0.0143 | -0.0428 | 0.1668 | 0.0186 | 0.1637 | 6.3403 | -5.355 | 0.9209 | 38 | 5.5493 | -2.0913 | -0.818 | 3.0691 | 1.0014 | 0.793 | 0.0096 | 0.1828 | -0.1953 | -0.0752 | -0.073 | 0.1131 | 0.0021 | -0.0177 | 0.0634 | 0.083 | 0.007 | 0.0081 | 0.1454 | -0.003 | 0.1106 | 10.5866 | -12.1872 | 3.9949 | 39 | 7.0804 | 0.1489 | 1.0435 | 11.9188 | 1.1498 | 6.0423 | -0.1695 | 0.0737 | 0.4232 | 0.062 | 0.1414 | 0.6068 | -0.4464 | -0.2353 | 0.0281 | 0.0509 | 0.0109 | -0.0189 | 0.1465 | -0.0005 | 0.1667 | 0.5393 | -0.8107 | 10.3528 | 40 | 17.2694 | -7.6649 | -4.5894 | 11.0172 | 5.6713 | 2.9603 | -0.1361 | -0.3062 | -0.6376 | -0.055 | 0.1276 | 0.0237 | -0.0211 | 0.088 | 0.0085 | 0.0346 | -0.0042 | 0.0077 | 0.1286 | 0.004 | 0.1419 | 10.5371 | -17.9459 | 7.9407 | 41 | 18.4856 | -11.2967 | -3.7375 | 19.7532 | -2.3197 | 4.6851 | 0.2457 | 1.2748 | -0.7099 | -1.691 | -0.5354 | 1.0505 | 1.2894 | -0.7247 | 0.2897 | 0.4659 | -0.1276 | 0.0228 | 0.2556 | -0.0899 | 0.2092 | 4.1122 | -22.4655 | 8.4025 | 42 | 1.2403 | 0.2646 | -0.1623 | 3.4555 | -0.3616 | 0.8106 | -0.0234 | 0.1244 | 0.1698 | -0.2618 | 0.0256 | 0.1208 | -0.0932 | -0.0108 | -0.0023 | 0.0606 | 0.0064 | -0.0198 | 0.13 | 0.0016 | 0.1469 | 8.72 | -1.4409 | 10.2524 | 43 | 12.6198 | 4.5016 | 2.6522 | 20.668 | -0.9654 | 17.3849 | 0.1342 | 0.2613 | -0.5594 | 0.0805 | -0.0998 | 0.3126 | 0.8743 | -0.1853 | -0.0345 | 0.0698 | -0.0182 | -0.0203 | 0.1345 | 0.0047 | 0.1934 | 4.3811 | -25.0125 | 15.7751 | 44 | 1.285 | 0.7612 | -0.1482 | 4.9225 | -2.0883 | 1.6002 | 0.0099 | 0.0074 | -0.0072 | -0.0436 | -0.0557 | -0.0027 | -0.0181 | -0.0099 | 0.0458 | 0.0198 | 0.0137 | 0.0005 | 0.106 | -0.005 | 0.1158 | 12.9932 | -10.6215 | 13.8007 | 45 | 13.5171 | 8.9009 | -0.6962 | 8.0682 | -2.913 | 41.2742 | -0.4894 | 1.2264 | -0.2865 | -1.2699 | 0.5029 | -0.2962 | -0.565 | 0.9074 | -0.0134 | 0.7225 | 0.0019 | -0.0025 | 0.3081 | 0.0492 | 0.136 | 15.0072 | -1.3949 | -3.8896 | 46 | 1.1922 | -0.0979 | 0.5355 | 2.005 | -2.3199 | 6.3752 | -0.0488 | 0.0081 | -0.0351 | 0.0077 | 0.0311 | -0.0813 | -0.0433 | -0.0136 | 0.0177 | 0.0144 | 0.0059 | 0.0051 | 0.0917 | -0.0133 | 0.1299 | 18.0354 | -11.4066 | 16.0164 | 47 | 2.1507 | -0.6457 | 2.6707 | 2.6604 | -3.6105 | 10.7839 | 0.0134 | -0.1249 | -0.1004 | 0.1092 | -0.0902 | -0.0768 | -0.0786 | 0.1554 | 0.0769 | 0.0077 | 0.0034 | 0.0063 | 0.1164 | -0.0107 | 0.151 | 22.9983 | -14.9081 | 21.2437 | 48 | 13.5519 | -5.6936 | 4.9195 | 3.3485 | -1.5962 | 11.7374 | 0.3535 | 0.9364 | -0.4791 | -0.6684 | 0.0135 | 0.4611 | -0.4013 | 0.0935 | -0.367 | 0.3384 | -0.1599 | -0.0997 | 0.2863 | 0.0897 | 0.2059 | 9.8695 | -8.4443 | -2.9266 |
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精密化 TLSグループ | ID | Refine-ID | Refine TLS-ID | Auth asym-ID | Auth seq-ID |
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1 | X-RAY DIFFRACTION | 1 | A214 - 222 | 2 | X-RAY DIFFRACTION | 2 | A223 - 236 | 3 | X-RAY DIFFRACTION | 3 | A237 - 248 | 4 | X-RAY DIFFRACTION | 4 | A49 - 54 | 5 | X-RAY DIFFRACTION | 5 | A55 - 83 | 6 | X-RAY DIFFRACTION | 6 | A84 - 88 | 7 | X-RAY DIFFRACTION | 7 | A89 - 96 | 8 | X-RAY DIFFRACTION | 8 | A97 - 103 | 9 | X-RAY DIFFRACTION | 9 | A104 - 115 | 10 | X-RAY DIFFRACTION | 10 | A116 - 120 | 11 | X-RAY DIFFRACTION | 11 | A121 - 128 | 12 | X-RAY DIFFRACTION | 12 | A129 - 133 | 13 | X-RAY DIFFRACTION | 13 | B213 - 235 | 14 | X-RAY DIFFRACTION | 14 | B236 - 242 | 15 | X-RAY DIFFRACTION | 15 | B243 - 248 | 16 | X-RAY DIFFRACTION | 16 | B49 - 54 | 17 | X-RAY DIFFRACTION | 17 | B55 - 79 | 18 | X-RAY DIFFRACTION | 18 | B80 - 84 | 19 | X-RAY DIFFRACTION | 19 | B85 - 100 | 20 | X-RAY DIFFRACTION | 20 | B101 - 105 | 21 | X-RAY DIFFRACTION | 21 | B106 - 115 | 22 | X-RAY DIFFRACTION | 22 | B116 - 120 | 23 | X-RAY DIFFRACTION | 23 | B121 - 135 | 24 | X-RAY DIFFRACTION | 24 | B136 - 143 | 25 | X-RAY DIFFRACTION | 25 | C213 - 221 | 26 | X-RAY DIFFRACTION | 26 | C222 - 227 | 27 | X-RAY DIFFRACTION | 27 | C228 - 236 | 28 | X-RAY DIFFRACTION | 28 | C237 - 248 | 29 | X-RAY DIFFRACTION | 29 | C50 - 79 | 30 | X-RAY DIFFRACTION | 30 | C80 - 84 | 31 | X-RAY DIFFRACTION | 31 | C85 - 99 | 32 | X-RAY DIFFRACTION | 32 | C100 - 104 | 33 | X-RAY DIFFRACTION | 33 | C105 - 115 | 34 | X-RAY DIFFRACTION | 34 | C116 - 120 | 35 | X-RAY DIFFRACTION | 35 | C121 - 129 | 36 | X-RAY DIFFRACTION | 36 | C130 - 143 | 37 | X-RAY DIFFRACTION | 37 | D213 - 222 | 38 | X-RAY DIFFRACTION | 38 | D223 - 233 | 39 | X-RAY DIFFRACTION | 39 | D234 - 240 | 40 | X-RAY DIFFRACTION | 40 | D241 - 248 | 41 | X-RAY DIFFRACTION | 41 | D49 - 54 | 42 | X-RAY DIFFRACTION | 42 | D55 - 79 | 43 | X-RAY DIFFRACTION | 43 | D80 - 84 | 44 | X-RAY DIFFRACTION | 44 | D85 - 96 | 45 | X-RAY DIFFRACTION | 45 | D97 - 103 | 46 | X-RAY DIFFRACTION | 46 | D104 - 115 | 47 | X-RAY DIFFRACTION | 47 | D116 - 129 | 48 | X-RAY DIFFRACTION | 48 | D130 - 134 | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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