CHAIN A AND B POLYSACCHARIDE BLOOD GROUP A TYPE 1 HEXASACCHARIDE FROM SUS SCROFA DOMESTICA ...CHAIN A AND B POLYSACCHARIDE BLOOD GROUP A TYPE 1 HEXASACCHARIDE FROM SUS SCROFA DOMESTICA SACCHARIDE ACQUIRED FROM ELICITYL (FRANCE)
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 2.25 Å3/Da / 溶媒含有率: 45 % / 解説: NONE
結晶化
詳細: 0.17 M AMMONIUM SULFATE, 25.5% (W/V) PEG 4000 AND 15% (V/V) GLYCEROL
解像度: 2→19.98 Å / Cor.coef. Fo:Fc: 0.939 / Cor.coef. Fo:Fc free: 0.918 / SU B: 8.103 / SU ML: 0.115 / 交差検証法: THROUGHOUT / ESU R: 0.2 / ESU R Free: 0.173 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. SIDE CHAINS WITH POOR OR MISSING ELECTRON DENSITY WERE MODELLED IN MOST LIKELY CONFORMER, WITH OCCUPANCY SET TO 0
Rfactor
反射数
%反射
Selection details
Rfree
0.2387
977
5 %
RANDOM
Rwork
0.1939
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obs
0.19622
18561
100 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK