SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AA" IN EACH CHAIN ON SHEET RECORDS BELOW ... SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AA" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 8-STRANDED BARREL THIS IS REPRESENTED BY A 9-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL. THE SHEETS PRESENTED AS "BA" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 8-STRANDED BARREL THIS IS REPRESENTED BY A 9-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL.
Resolution: 2.25→55.64 Å / Cor.coef. Fo:Fc: 0.933 / Cor.coef. Fo:Fc free: 0.889 / SU B: 9.538 / SU ML: 0.237 / Cross valid method: THROUGHOUT / ESU R: 0.351 / ESU R Free: 0.274 / Stereochemistry target values: MAXIMUM LIKELIHOOD Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. U VALUES REFINED INDIVIDUALLY. RESIDUES A1, A22-28, A143-146, B1, B140-149 ARE DISORDERED AND NOT MODELED, RESIDUES A247, B247-250 ARE PART ...Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. U VALUES REFINED INDIVIDUALLY. RESIDUES A1, A22-28, A143-146, B1, B140-149 ARE DISORDERED AND NOT MODELED, RESIDUES A247, B247-250 ARE PART OF THE C-TERMINAL HIS-TAG LINKER AND VISIBLE AND MODELED
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.30263
957
3.9 %
RANDOM
Rwork
0.23556
-
-
-
obs
0.23813
23607
99.42 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.4 Å / Solvent model: MASK