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- PDB-408d: STRUCTURAL BASIS FOR RECOGNITION OF A-T AND T-A BASE PAIRS IN THE... -
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Open data
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Basic information
Entry | Database: PDB / ID: 408d | ||||||||||||||||||
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Title | STRUCTURAL BASIS FOR RECOGNITION OF A-T AND T-A BASE PAIRS IN THE MINOR GROOVE OF B-DNA | ||||||||||||||||||
![]() | DNA (5'-D(*![]() DNA / DRUG IN THE DNA MINOR GROOVE | Function / homology | IMIDAZOLE-PYRROLE POLYAMIDE / DNA | ![]() Method | ![]() ![]() Kielkopf, C.L. / White, S. / Szewczyk, J.W. / Turner, J.M. / Baird, E.E. / Dervan, P.B. / Rees, D.C. | ![]() ![]() Title: A structural basis for recognition of A.T and T.A base pairs in the minor groove of B-DNA. Authors: Kielkopf, C.L. / White, S. / Szewczyk, J.W. / Turner, J.M. / Baird, E.E. / Dervan, P.B. / Rees, D.C. History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 25.4 KB | Display | ![]() |
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PDB format | ![]() | 17.2 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Summary document | ![]() | 472.9 KB | Display | ![]() |
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Full document | ![]() | 481.5 KB | Display | |
Data in XML | ![]() | 3.4 KB | Display | |
Data in CIF | ![]() | 4.7 KB | Display | |
Arichive directory | ![]() ![]() | HTTPS FTP |
-Related structure data
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Links
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Assembly
Deposited unit | ![]()
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1 |
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Unit cell |
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Components
#1: DNA chain | Mass: 3045.004 Da / Num. of mol.: 2 Source method: isolated from a genetically manipulated source #2: Chemical | #3: Water | ChemComp-HOH / | |
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-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 2.72 Å3/Da / Density % sol: 54.82 % | ||||||||||||||||||||||||||||
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Crystal grow | Temperature: 293 K / Method: vapor diffusion, hanging drop / pH: 7.5 Details: pH 7.50, VAPOR DIFFUSION, HANGING DROP, temperature 293.00K | ||||||||||||||||||||||||||||
Components of the solutions |
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Crystal grow | *PLUS Method: unknown | ||||||||||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Mean temperature: 103 K |
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Diffraction source | Source: ![]() |
Detector | Type: RIGAKU / Detector: IMAGE PLATE / Date: Nov 15, 1997 |
Radiation | Scattering type: x-ray |
Radiation wavelength | Relative weight: 1 |
Reflection | Resolution: 2.1→16 Å / Num. all: 3417 / Num. obs: 3417 / % possible obs: 91 % / Observed criterion σ(F): 0 / Observed criterion σ(I): 0 / Redundancy: 3.6 % / Rmerge(I) obs: 0.038 |
Reflection | *PLUS % possible obs: 91.6 % / Num. measured all: 12267 |
Reflection shell | *PLUS Highest resolution: 2.1 Å / Lowest resolution: 2.18 Å / % possible obs: 82.9 % / Rmerge(I) obs: 0.179 / Mean I/σ(I) obs: 4.1 |
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Processing
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Refinement | Resolution: 2.1→20 Å / σ(F): 0
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Refinement step | Cycle: LAST / Resolution: 2.1→20 Å
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Refine LS restraints |
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Xplor file | Serial no: 1 / Param file: NOC2ENDO.PARAM / Topol file: IPPP_NODIH.PAR | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Software | *PLUS Name: ![]() | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Refinement | *PLUS | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Solvent computation | *PLUS | ||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Displacement parameters | *PLUS |