Mass: 18.015 Da / Num. of mol.: 318 / Source method: isolated from a natural source / Formula: H2O
Sequence details
INITIATOR METHIONINE IS CLEAVED FROM THE MATURE WRBA PROTEIN AND RESIDUE NUMBERING IN THE STRUCTURE ...INITIATOR METHIONINE IS CLEAVED FROM THE MATURE WRBA PROTEIN AND RESIDUE NUMBERING IN THE STRUCTURE FOLLOWS AS DEFINED IN WOLFOVA ET, AL. WITH THE FIRST RESIDUE AN ALANINE.
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 1.85 Å3/Da / Density % sol: 34 % / Description: NONE
Crystal grow
Details: WRBA-FAD AT A CONCENTRATION OF 5 MG/ML IN 20 MM TRIS PH 6.5 CRYSTALLYZED AGAINST WELL CONTAINING 28% PEG 3350 AND 0.05 M BIS-TRIS-HCL, PH 6.5.
Resolution: 1.2→21.46 Å / Cor.coef. Fo:Fc: 0.975 / Cor.coef. Fo:Fc free: 0.966 / SU B: 1.166 / SU ML: 0.024 / Cross valid method: THROUGHOUT / ESU R: 0.041 / ESU R Free: 0.039 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.1704
4864
5 %
RANDOM
Rwork
0.1473
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obs
0.14846
92773
96.37 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK