ソフトウェア 名称 バージョン 分類 NB MOLREP位相決定 Show PHENIX1.6.1_357精密化 Show PDB_EXTRACT3.1 データ抽出 Show
精密化 構造決定の手法 : 分子置換 / 解像度 : 3→40.96 Å / Occupancy max : 1 / Occupancy min : 0.62 / SU ML : 0.31 / σ(F) : 0.07 / 立体化学のターゲット値 : MLRfactor 反射数 %反射 Rfree 0.25 1873 4.18 % Rwork 0.212 - - obs 0.213 44764 76.8 % all - 44764 -
溶媒の処理 減衰半径 : 0.9 Å / VDWプローブ半径 : 1.11 Å / 溶媒モデル : FLAT BULK SOLVENT MODEL / Bsol : 59.84 Å2 / ksol : 0.3 e/Å3 原子変位パラメータ Biso mean : 117.89 Å2 Baniso -1 Baniso -2 Baniso -3 1- 36.0326 Å2 0 Å2 -0 Å2 2- - 1.1962 Å2 0 Å2 3- - - -37.2288 Å2
精密化ステップ サイクル : LAST / 解像度 : 3→40.96 Åタンパク質 核酸 リガンド 溶媒 全体 原子数 16517 990 20 0 17527
拘束条件 Refine-ID タイプ Dev ideal 数 X-RAY DIFFRACTION f_bond_d0.01 18018 X-RAY DIFFRACTION f_angle_d1.448 24627 X-RAY DIFFRACTION f_dihedral_angle_d19.576 6811 X-RAY DIFFRACTION f_chiral_restr0.101 2716 X-RAY DIFFRACTION f_plane_restr0.006 2984
Refine LS restraints NCS Ens-ID Dom-ID Auth asym-ID 数 Refine-ID タイプ Rms dev position (Å)1 1 A3241 X-RAY DIFFRACTION POSITIONAL1 2 B3241 X-RAY DIFFRACTION POSITIONAL0.039 1 3 C3233 X-RAY DIFFRACTION POSITIONAL0.041 1 4 D3241 X-RAY DIFFRACTION POSITIONAL0.043 1 5 E3241 X-RAY DIFFRACTION POSITIONAL0.041
LS精密化 シェル 解像度 (Å)Rfactor Rfree Num. reflection Rfree Rfactor Rwork Num. reflection Rwork Refine-ID % reflection obs (%)3.0001-3.0812 0.3601 51 0.2814 1151 X-RAY DIFFRACTION 27 3.0812-3.1719 0.3134 66 0.281 1475 X-RAY DIFFRACTION 35 3.1719-3.2742 0.2837 83 0.2847 1991 X-RAY DIFFRACTION 47 3.2742-3.3912 0.3204 107 0.2796 2596 X-RAY DIFFRACTION 61 3.3912-3.5269 0.2965 145 0.2563 3186 X-RAY DIFFRACTION 75 3.5269-3.6873 0.2925 158 0.2378 3581 X-RAY DIFFRACTION 84 3.6873-3.8815 0.3125 166 0.228 3826 X-RAY DIFFRACTION 89 3.8815-4.1245 0.2167 175 0.1968 3908 X-RAY DIFFRACTION 92 4.1245-4.4426 0.2443 180 0.1939 4032 X-RAY DIFFRACTION 95 4.4426-4.8891 0.2083 180 0.1693 4152 X-RAY DIFFRACTION 96 4.8891-5.595 0.2228 179 0.1738 4219 X-RAY DIFFRACTION 97 5.595-7.0433 0.2424 188 0.1965 4292 X-RAY DIFFRACTION 98 7.0433-40.9628 0.2352 195 0.2126 4482 X-RAY DIFFRACTION 98
精密化 TLS 手法 : refined / Refine-ID : X-RAY DIFFRACTION
大きな表を表示 (25 x 65) 大きな表を隠す ID L11 (°2 )L12 (°2 )L13 (°2 )L22 (°2 )L23 (°2 )L33 (°2 )S11 (Å °)S12 (Å °)S13 (Å °)S21 (Å °)S22 (Å °)S23 (Å °)S31 (Å °)S32 (Å °)S33 (Å °)T11 (Å2 )T12 (Å2 )T13 (Å2 )T22 (Å2 )T23 (Å2 )T33 (Å2 )Origin x (Å)Origin y (Å)Origin z (Å)1 3.4048 1.0232 3.6184 2.0765 1.8915 6.0632 -0.076 1.2598 -0.0579 -1.3889 0.0674 -0.4516 -0.4172 2.0011 -0.2022 0.5218 0.2889 0.2305 0.47 -0.2235 0.7154 -18.6661 56.2558 76.0384 2 0.1818 -0.2937 -0.1685 -0.5496 0.2808 0.8227 1.3176 -0.4111 1.1062 -0.7803 -1.0612 -0.7559 -0.4918 0.0348 -0.0192 1.3737 0.7973 0.3149 0.5938 0.3842 1.1332 -51.2197 45.0333 51.3724 3 0.5603 -0.0204 0.1802 0.6429 -0.1091 0.0526 0.0354 1.1312 0.1515 -1.0996 0.6283 -0.2917 0.6099 -0.9392 -0.0003 1.1778 0.3472 0.1544 1.6048 0.3716 0.7711 -50.6774 31.7103 30.9363 4 0.4382 0.6289 -0.0786 1.0714 -0.833 0.7656 -0.5303 1.027 0.6971 -1.2055 0.767 1.0701 1.0975 -2.0083 0.0096 0.6796 0.1365 0.1933 1.7075 0.4205 1.1724 -64.3645 33.9942 51.2917 5 0.7031 0.2626 1.024 0.3571 0.5939 1.1903 0.5411 1.5815 0.3269 1.8653 -0.2335 1.1775 0.0743 -2.2843 -0.0288 1.3818 0.2173 -0.2552 1.4307 0.3542 0.9798 -51.3536 33.3291 26.7896 6 -0.1068 0.2559 -0.3412 -0.1072 -0.2654 2.0415 0.3147 -0.3281 0.1371 -0.0712 0.6865 -0.6157 0.0592 -0.055 -0.0022 1.0833 0.1167 0.3945 1.0925 0.4252 0.9188 -40.7462 21.103 39.0113 7 0.4468 0.6708 -1.07 1.1223 -0.3833 0.4753 0.0884 0.6857 1.644 -0.3598 0.6537 0.9348 -0.2695 -2.0104 -0.0015 0.4991 0.3089 -0.0207 0.8978 0.3952 0.767 -47.5915 31.3278 44.6848 8 -0.5747 3.3534 2.6776 -1.1317 2.8139 0.8711 0.0182 -0.0222 -0.3028 -0.9495 0.7676 0.1615 0.239 -0.7667 0.1071 0.3519 0.5631 0.2745 0.787 0.241 0.6467 -45.7442 31.515 62.7868 9 2.5182 -0.1559 1.0162 0.6094 -0.9417 2.1667 0.5858 0.5204 0.7044 -0.0803 -0.3789 -0.1636 -0.8523 -0.4765 0.0001 0.5759 0.3745 0.275 0.7685 0.1701 0.637 -31.6323 26.1127 70.7253 10 4.1164 2.7736 -1.4569 1.9866 -1.4031 1.3142 -0.4315 4.5696 0.3534 -1.5676 1.7892 0.6081 0.6408 -1.7791 0.0351 0.8155 -0.0123 0.2996 1.0573 0.1401 0.7581 -52.3865 5.2707 86.1075 11 0.0602 -0.0095 -0.1585 0.1215 -0.0378 0.2991 0.5514 2.2288 -1.4105 -0.2413 -1.799 1.1287 -0.9297 -1.3725 -0.0006 0.7116 -0.2889 0.3655 1.5727 0.1406 1.4386 -37.9255 12.3319 98.5466 12 1.4505 -0.7152 1.488 3.2853 -2.4823 2.8404 -0.098 -0.4636 -0.4109 0.0453 0.0388 -0.1796 0.7455 0.0605 0.0005 0.5244 0.2336 0.346 0.6637 0.212 0.8779 -27.0178 20.769 78.0345 13 1.2672 -0.5224 0.5086 0.5562 -0.3233 1.2547 0.1411 1.0472 0.4366 0.234 -0.6861 -0.0257 -0.5727 1.0123 -0.0178 0.8329 -0.1632 0.1342 0.5365 -0.1488 0.7237 18.2053 56.1738 76.1182 14 0.5841 -0.2731 -0.3914 0.0715 0.2445 0.2573 -0.1188 -0.1166 0.7099 0.2711 -0.1839 -0.742 -0.1033 1.3803 0.0002 1.1958 -0.2031 0.2719 0.4325 0.137 1.1753 -14.6931 66.007 51.3262 15 0.4907 -1.3537 0.6405 1.4654 -0.7433 0.3716 0.3755 1.0682 0.2664 -0.439 0.0183 0.6577 -0.7449 0.1516 0.0001 1.1444 0.2355 0.1804 1.4082 0.1648 0.863 -21.9567 54.8288 30.8888 16 0.0761 -0.4212 -0.0874 0.3948 0.015 0.0245 -0.8524 0.1298 0.8149 1.197 0.4743 0.3116 -0.1534 -1.0133 0.0008 0.9155 0.3754 0.2594 1.1311 0.023 1.3614 -31.3504 64.8738 50.7918 17 0.8573 -0.1279 0.5256 0.1546 -0.4511 0.3382 3.1238 1.6523 0.9217 0.5331 -1.4446 0.4859 -0.6736 -1.1785 0.0192 1.2659 0.0146 0.3744 0.7933 0.3996 0.9758 -21.6783 55.8897 26.0768 18 0.897 0.1046 -0.36 0.9247 -1.098 1.273 0.6272 -0.2135 0.4573 -0.1962 0.1127 -0.8453 1.2315 0.546 0.0069 1.0833 0.3678 0.5601 0.8743 0.103 0.7855 -18.8352 40.9878 41.4324 19 1.958 1.6286 -0.3615 3.9856 -4.6505 6.6665 -1.5318 2.8854 -2.2368 -2.1516 1.8579 0.7333 2.3531 -0.3234 0.9071 -0.1108 0.387 0.4911 0.5481 0.1022 0.9283 -19.465 39.6581 34.5729 20 0.8431 1.2548 0.3756 -1.4961 0.4095 1.4875 0.0611 0.2302 0.2407 0.2582 0.1524 0.2875 -0.4016 0.0235 -0.0004 0.8505 0.3345 0.2412 0.403 0.1027 0.6547 -19.0262 52.4081 58.4187 21 0.5025 1.5127 -0.2356 1.6029 -0.0021 0.3819 0.2888 0.3698 0.3001 -0.4317 -0.1539 -0.378 -0.363 0.4255 0.0005 0.6772 0.2405 0.1981 0.4399 0.0039 0.6931 -9.9131 39.2517 70.7502 22 2.0326 -0.6525 -2.0791 0.4316 0.6883 2.2582 1.31 2.5636 0.0051 -2.0067 0.2409 -0.2416 -1.9085 -2.1512 -0.0044 0.8101 0.1081 0.3927 0.6724 0.2186 0.9417 -38.5791 34.5468 86.4976 23 0.498 0.2068 -0.6183 0.162 -0.3706 -0.0312 1.0661 0.599 -1.0509 -0.362 -1.2745 0.1893 0.3877 1.365 0.0006 1.2914 0.3914 0.4834 0.8833 0.2921 1.0062 -17.1709 37.5115 90.5003 24 2.9861 0.1612 -1.8532 2.3146 -1.1023 1.3112 -0.0696 -0.1604 -0.7239 0.5007 0.5028 -0.4235 0.6484 0.0834 0.0098 0.5898 0.2735 0.1774 0.4131 0.0387 0.7911 -7.126 29.9229 74.6885 25 1.2586 -0.1783 -0.5074 0.504 0.0102 0.5878 0.567 0.6186 0.3344 -0.1149 -0.7462 0.0017 0.7979 0.5437 -0.0048 0.8024 -0.3169 -0.1279 0.6525 -0.171 0.8516 48.14 35.008 76.0621 26 0.0331 -0.363 0.6043 0.4002 -0.3561 0.3485 -0.2709 -0.5277 -0.2993 0.1591 0.7103 -1.1009 -1.8473 0.686 -0.0037 1.2835 -0.5985 0.393 0.7162 -0.2175 0.9837 27.0014 62.1301 51.3454 27 0.2132 -0.1268 -1.8119 1.149 -0.8739 1.6463 1.0102 1.4912 0.9482 -0.3303 -0.2398 0.1996 -0.4825 -0.3352 0.0002 1.2707 0.0193 0.1662 1.2639 0.1391 0.8172 14.5926 57.2781 30.8982 28 0.9253 0.1347 0.6684 -0.0025 0.049 0.3833 0.3877 -0.5466 0.7454 -0.1065 0.341 -0.5415 -1.468 -0.836 0.0004 1.4813 0.294 0.6328 0.79 0.1213 1.1847 12.2928 70.9841 51.2396 29 0.2347 -0.1857 0.7676 0.8601 0.0668 1.2412 1.0435 -0.9438 0.6968 -1.6338 -0.0339 -0.4624 -0.6496 -1.9242 -0.0114 1.0164 -0.0086 0.32 1.1983 0.376 0.8598 15.9126 58.4323 26.7523 30 0.9963 0.4908 0.2919 0.3321 -0.5122 1.5166 0.4975 -0.0402 -1.1406 -0.0898 0.0541 -0.5329 2.4789 -0.9597 0.0714 0.9671 -0.0209 0.5119 0.7736 -0.0781 0.6721 9.1288 44.155 41.4102 31 0.9129 -0.2111 0.2519 0.2843 -0.5378 0.4947 0.714 1.2393 -0.3228 0.5233 0.4334 1.4236 -0.4574 -1.5725 0.0295 0.9528 0.0484 0.7068 1.2777 0.2634 1.0835 7.9265 43.6932 34.8062 32 1.5892 -1.282 -1.4825 -0.1766 0.4769 1.4955 0.497 0.3209 0.4858 -0.2752 0.0104 0.1526 -0.6576 0.0028 -0.0013 1.1367 -0.2107 0.255 0.4856 0.0147 0.7825 15.5966 53.5344 58.4177 33 1.638 -0.0685 -0.5233 1.4577 0.2208 1.9148 0.1767 0.3972 -0.0293 -1.0596 0.005 -0.3683 -0.4796 0.376 -0.0001 0.8886 -0.1026 0.1687 0.2964 -0.0653 0.6233 15.4105 37.4957 70.7121 34 1.1008 -1.6633 -0.3088 4.1411 -0.6446 0.4889 0.7226 0.5276 -0.5111 -2.5568 -0.1731 0.292 -0.0097 -1.3493 0.0645 0.436 0.1568 0.3064 0.6506 -0.2049 0.5949 -10.6733 50.2278 86.5 35 0.1283 0.0788 0.4011 -0.0892 0.257 0.6754 1.1796 -0.3956 0.6777 -1.729 -0.3057 -0.7826 -1.0799 1.5074 -0.0001 1.3572 0.2054 0.4678 0.5124 -0.0655 0.8736 9.5871 40.3091 89.63 36 3.0833 -0.1801 -2.363 1.071 1.0771 1.6921 0.221 0.0722 -0.6895 0.1289 -0.0098 0.0084 0.2317 -0.7019 -0.0005 0.7949 -0.0544 0.1637 0.316 -0.0375 0.8101 12.2736 28.2724 74.6312 37 0.1851 -0.2213 -0.1378 0.2256 -0.3152 0.259 -0.0933 0.1664 0.3704 0.4504 -0.9477 -1.2685 0.1277 0.3831 -0.0011 0.5876 -0.0649 -0.3382 1.2629 -0.2013 0.8372 60.5387 -1.2704 77.7911 38 -0.2572 0.2717 0.1842 1.7466 -0.305 0.0147 0.3405 -0.1001 0.0075 1.1536 -1.0077 -0.6933 0.235 2.0038 -0.0106 0.2534 0.0162 -0.0607 2.0172 -0.2915 1.0286 58.5365 33.034 52.1109 39 0.7551 0.6924 -0.3256 0.449 0.063 0.404 0.1839 0.9742 0.2758 -1.4627 -0.1024 -0.0268 0.2744 0.8731 -0.0005 1.264 -0.3048 0.2261 1.2753 -0.0056 0.7586 45.6391 37.8545 30.8009 40 0.441 -0.1357 0.5904 -0.1366 -0.0178 0.5369 0.6232 0.2358 1.1144 -0.1014 -0.8975 -1.6696 -2.3165 0.8753 -0.0003 1.6474 -0.249 0.101 0.7663 -0.0879 1.3932 52.0672 50.058 50.6694 41 1.1427 1.8554 0.1062 4.2042 1.3145 1.4136 -2.3322 0.3012 0.6198 -2.4018 2.1554 0.7949 -1.3135 -0.1578 -0.0317 0.8498 -0.1898 0.5547 1.5402 -0.11 0.9128 45.7781 38.1099 26.5232 42 0.7073 0.3559 0.0258 0.5394 -1.0495 1.1681 0.0575 -0.2555 -0.7794 0.0083 0.253 0.262 1.282 -0.2318 0.0013 0.7386 -0.1887 0.0985 0.8813 -0.3155 0.6693 33.5609 29.8282 41.839 43 6.2537 -4.4188 -2.7997 6.3896 1.3837 1.0811 3.1161 2.1139 2.2881 -1.494 -3.0609 -0.5502 -0.2753 -1.8422 -0.0839 0.921 -0.0091 0.4045 0.6233 -0.2381 1.1394 32.1214 30.2219 34.2237 44 -0.3098 -1.4932 0.4898 0.8872 -1.6495 2.6039 0.1893 0.0737 0.2186 -0.1032 -0.0925 -0.1858 0.0706 0.4101 -0.0003 0.4895 -0.4451 0.1645 0.721 -0.1481 0.685 44.3738 34.3293 58.3352 45 2.1129 -0.0451 -0.4727 2.6161 0.4313 1.4387 -0.0239 0.8041 -0.4423 -0.8711 0.0261 -0.2524 0.0438 1.1665 -0.0063 0.4168 -0.4413 -0.0496 0.5084 -0.2515 0.6678 34.9712 21.4161 70.7071 46 1.6658 -2.4362 -2.0176 4.2886 3.2864 2.6136 1.7707 2.1788 -0.7349 -4.1166 -0.2611 -0.0409 -2.7284 -0.377 -0.03 1.0152 -0.0178 0.24 0.7068 -0.326 0.8428 20.6817 47.2391 84.999 47 0.6112 -0.1467 -0.0417 0.4165 0.1145 0.5266 -0.034 -0.5741 0.8731 -1.5618 0.3475 -0.7013 1.5057 -0.2339 -0.0039 1.128 -0.298 0.113 1.0156 -0.0019 1.1177 24.5783 33.2495 96.1184 48 3.3557 -0.1846 -1.3206 0.5977 -0.3436 2.5879 0.2824 -0.0668 -0.4801 0.1485 -0.1302 0.3099 0.0136 -0.6015 -0.0004 0.7291 -0.0743 0.0403 0.5294 -0.1778 0.7247 28.5813 18.4981 77.8843 49 1.2014 -1.1867 0.049 0.8798 0.0371 0.0685 -0.3638 0.6151 0.0241 -1.3101 -0.7959 0.3472 -1.19 0.2457 0.0009 0.9146 0.2756 0.3603 1.0431 0.0185 0.9087 -48.8788 34.7845 76.1426 50 0.2722 0.0802 -0.4787 1.0954 -0.2426 0.4935 1.1645 0.0508 -0.0923 -0.3239 0.1096 -0.0002 0.104 -0.2139 -0.0009 0.9206 0.5446 0.0474 1.4629 0.336 1.1022 -68.4618 6.4053 51.5385 51 0.5336 0.2239 0.1386 0.3987 0.3744 0.3664 -0.053 0.3977 -0.0373 -2.2045 0.0869 0.4647 -0.0069 -0.5716 0.001 1.9272 -0.2891 -0.467 2.1086 0.3513 1.0207 -60.1972 -3.893 31.0154 52 0.2852 -0.1265 0.4857 0.1777 -0.1496 0.3265 1.0837 -1.3023 -1.0584 -1.2849 -0.4457 0.1282 2.993 -0.4337 0.0048 1.5854 -0.319 -0.2671 1.4438 0.5041 1.6602 -72.416 -9.8129 51.0332 53 -0.0832 -0.0539 0.1065 0.1911 -0.2236 0.1329 -0.2867 0.0687 -0.119 1.2626 2.3246 0.7423 1.9168 -1.2296 -0.0039 1.394 0.2893 -0.3166 1.48 0.2247 1.2044 -61.1688 -3.3011 26.2164 54 0.4441 0.6317 1.2982 -0.0486 0.4395 1.2802 0.1031 -0.1702 0.2475 0.0356 -0.0377 -0.0369 -0.8325 -0.0258 0.0009 1.0942 0.017 0.0205 0.9286 0.546 0.8503 -45.6076 -6.4132 38.8724 55 -0.128 -0.1222 -0.0357 0.1963 -0.2611 0.0759 -1.1184 -0.1565 0.4338 -1.9279 0.766 0.9898 0.5986 -0.7077 0.0031 0.7107 -0.1622 -0.19 1.3127 0.2062 0.9546 -57.4016 -2.3942 44.7492 56 -0.784 1.2483 2.28 1.7298 1.3312 1.9331 0.3234 0.0108 -0.0739 -0.379 -0.0538 0.0909 0.3507 -0.6898 -0.0011 0.3218 0.0114 0.0322 1.3123 0.3053 0.8251 -55.9091 -1.1996 62.8419 57 1.8812 0.8879 0.2654 1.5219 0.1683 0.4642 0.0696 0.6857 0.6235 -0.4001 -0.0801 -0.0419 0.0034 -0.7504 -0.0004 0.3056 -0.0505 0.0818 0.7936 0.2458 0.7213 -41.3095 2.8796 70.6984 58 0.092 -0.17 -0.1631 0.1021 0.1065 0.0364 -0.8669 0.8369 0.2042 -3.2179 1.0665 -0.8693 1.0926 -0.4919 -0.0057 0.9397 -0.1505 0.0967 0.8518 0.2613 0.7427 -45.1548 -26.3638 85.0153 59 0.3131 -0.2145 -0.3047 0.1259 0.2018 0.3097 0.1603 0.9991 -0.4777 1.1067 1.0534 0.5251 -1.8509 -0.1946 -0.002 1.1096 -0.1903 -0.0084 0.8302 0.3456 1.3524 -39.5951 -13.1042 96.703 60 2.5771 -2.0173 1.7499 1.5928 -1.2743 2.0321 -0.0942 -0.3434 0.3603 0.2269 0.1885 -0.619 1.0216 0.3896 0.0041 0.313 -0.2025 0.1796 0.6379 0.0912 0.6707 -34.3563 1.3908 77.7943 61 2.2229 -1.7982 0.3772 0.4026 -1.1333 -0.0321 0.81 1.3105 -0.6765 -0.8583 -0.5491 0.3886 -0.6592 0.5386 -0.0016 1.4582 -0.2839 0.2726 1.3635 -0.1755 0.7683 28.2339 33.0209 53.8781 62 0.1923 -0.1883 -0.2163 0.08 0.0825 0.0592 -0.1528 1.7949 0.6443 -1.0012 0.8699 -0.4697 1.6517 1.8683 -0.0073 1.6992 0.02 0.3569 1.3497 0.0435 0.8066 -3.8244 49.32 52.6803 63 0.6308 1.2135 -0.1968 1.1638 -0.0596 -0.1649 -2.0372 0.3248 -0.2326 0.2649 1.3424 -0.2117 0.0342 0.0355 0.0027 1.4331 0.5142 0.2452 1.3366 0.287 0.7703 -25.505 37.9916 53.4721 64 0.1124 -0.1646 -0.1651 0.9984 -0.3864 0.3942 -0.8091 -1.2919 -0.6641 -1.4045 0.3992 -0.636 -0.3686 0.4994 0.0063 1.3146 0.2662 0.1013 1.6326 0.4611 0.9328 -43.493 16.127 53.5521 65 0.2597 -0.4971 -0.1563 0.5689 0.0486 0.2669 1.7654 -2.4313 -1.4838 0.7293 -0.7661 -2.5865 1.3835 0.3783 -0.0055 1.3403 -0.4707 -0.0954 2.0549 0.3823 0.9319 -43.797 -5.5934 53.0827
精密化 TLSグループ 大きな表を表示 (4 x 65) 大きな表を隠す ID Refine-ID Refine TLS-ID Selection details 1 X-RAY DIFFRACTION 1 (CHAIN A AND RESID 2:22)2 X-RAY DIFFRACTION 2 (CHAIN A AND RESID 23:45)3 X-RAY DIFFRACTION 3 (CHAIN A AND RESID 46:81)4 X-RAY DIFFRACTION 4 (CHAIN A AND RESID 82:109)5 X-RAY DIFFRACTION 5 (CHAIN A AND RESID 110:132)6 X-RAY DIFFRACTION 6 (CHAIN A AND RESID 133:177)7 X-RAY DIFFRACTION 7 (CHAIN A AND RESID 178:207)8 X-RAY DIFFRACTION 8 (CHAIN A AND RESID 208:290)9 X-RAY DIFFRACTION 9 (CHAIN A AND RESID 291:342)10 X-RAY DIFFRACTION 10 (CHAIN A AND RESID 343:355)11 X-RAY DIFFRACTION 11 (CHAIN A AND RESID 356:367)12 X-RAY DIFFRACTION 12 (CHAIN A AND RESID 368:422)13 X-RAY DIFFRACTION 13 (CHAIN B AND RESID 2:22)14 X-RAY DIFFRACTION 14 (CHAIN B AND RESID 23:45)15 X-RAY DIFFRACTION 15 (CHAIN B AND RESID 46:81)16 X-RAY DIFFRACTION 16 (CHAIN B AND RESID 82:110)17 X-RAY DIFFRACTION 17 (CHAIN B AND RESID 111:132)18 X-RAY DIFFRACTION 18 (CHAIN B AND