温度: 298 K / 手法: 蒸気拡散法, ハンギングドロップ法 / pH: 7.5 詳細: Protein concentration 13.5 mg/mL in 2.5 mM HEPES pH 7.5, Precipitant 0.02 M MgCl2, 22% polyacrylic acid 5100 in 0.1 M HEPES at pH 7.5, 3mM ornithine in mother liquor used to soak the crystal, ...詳細: Protein concentration 13.5 mg/mL in 2.5 mM HEPES pH 7.5, Precipitant 0.02 M MgCl2, 22% polyacrylic acid 5100 in 0.1 M HEPES at pH 7.5, 3mM ornithine in mother liquor used to soak the crystal, VAPOR DIFFUSION, HANGING DROP, temperature 298K
解像度: 2.4→50 Å / Cor.coef. Fo:Fc: 0.93 / Cor.coef. Fo:Fc free: 0.869 / SU B: 8.66 / SU ML: 0.198 / 交差検証法: THROUGHOUT / ESU R: 0.373 / ESU R Free: 0.269 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.26695
1887
5 %
RANDOM
Rwork
0.20955
-
-
-
obs
0.21241
35958
99.1 %
-
all
-
35958
-
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK