Arachidonate production from DAG / acylglycerol catabolic process / Acyl chain remodeling of DAG and TAG / アシルグリセロールリパーゼ / monoacylglycerol catabolic process / triglyceride catabolic process / regulation of endocannabinoid signaling pathway / acylglycerol lipase activity / arachidonic acid metabolic process / regulation of sensory perception of pain ...Arachidonate production from DAG / acylglycerol catabolic process / Acyl chain remodeling of DAG and TAG / アシルグリセロールリパーゼ / monoacylglycerol catabolic process / triglyceride catabolic process / regulation of endocannabinoid signaling pathway / acylglycerol lipase activity / arachidonic acid metabolic process / regulation of sensory perception of pain / lysophospholipase activity / Triglyceride catabolism / regulation of signal transduction / lipid metabolic process / fatty acid biosynthetic process / regulation of inflammatory response / 炎症 / endoplasmic reticulum membrane / protein homodimerization activity / 生体膜 / 細胞膜 / 細胞質基質 類似検索 - 分子機能
解像度: 2.2→2.3 Å / % possible obs: 86 % / 冗長度: 4.5 % / Mean I/σ(I) obs: 3.86 / Num. measured obs: 4066 / Rsym value: 0.4 / % possible all: 86.3
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解析
ソフトウェア
名称
バージョン
分類
REFMAC
5.2.0019
精密化
ADSC
Quantum
データ収集
XDS
データ削減
XSCALE
データスケーリング
PHASER
位相決定
精密化
構造決定の手法: 分子置換 開始モデル: a partial/incomplete model of PDB entries obtained by other methods 解像度: 2.2→43.02 Å / Cor.coef. Fo:Fc: 0.946 / Cor.coef. Fo:Fc free: 0.928 / 交差検証法: THROUGHOUT / σ(F): 0 / ESU R: 0.228 / ESU R Free: 0.187 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
反射数
%反射
Selection details
Rfree
0.22889
1896
5 %
RANDOM
Rwork
0.19207
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obs
0.19392
35779
97.93 %
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all
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37675
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK