Mass: 18.015 Da / Num. of mol.: 2 / Source method: isolated from a natural source / Formula: H2O
Compound details
ENGINEERED RESIDUE IN CHAIN A, G 18 TO U ENGINEERED RESIDUE IN CHAIN A, G 19 TO U ENGINEERED ...ENGINEERED RESIDUE IN CHAIN A, G 18 TO U ENGINEERED RESIDUE IN CHAIN A, G 19 TO U ENGINEERED RESIDUE IN CHAIN A, U 34 TO C ENGINEERED RESIDUE IN CHAIN A, A 94 TO G
Sequence details
MUTATIONS AT RESIDUES 18, 19, 34 AND 94. SEE REMARK 400
-
Experimental details
-
Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
-
Sample preparation
Crystal
Density Matthews: 2.31 Å3/Da / Density % sol: 64 % / Description: NONE
Crystal grow
pH: 7 Details: 40 MM NA-CACODYLATE (PH 7.0), 12 MM SPERMINE-HCL, 12% (V/V) MPD, 80 MM KCL.
Resolution: 2.9→57.62 Å / Cor.coef. Fo:Fc: 0.925 / Cor.coef. Fo:Fc free: 0.893 / Cross valid method: THROUGHOUT / ESU R Free: 0.573 / Stereochemistry target values: MAXIMUM LIKELIHOOD Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. U VALUES REFINED INDIVIDUALLY
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.32145
666
9.8 %
RANDOM
Rwork
0.26892
-
-
-
obs
0.27406
6121
92.52 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.4 Å / Solvent model: MASK