ENGINEERED RESIDUE IN CHAIN A, GLN 201 TO ALA ENGINEERED RESIDUE IN CHAIN B, GLN 201 TO ALA ...ENGINEERED RESIDUE IN CHAIN A, GLN 201 TO ALA ENGINEERED RESIDUE IN CHAIN B, GLN 201 TO ALA ENGINEERED RESIDUE IN CHAIN A, GLN 202 TO ALA ENGINEERED RESIDUE IN CHAIN B, GLN 202 TO ALA
非ポリマーの詳細
ETHYLENE GLYCOL (EDO): ETHYLENE GLYCOL WAS THE CRYOPROTECTANT GUANOSINE 5'-(TRIHYDROGEN DIPHOSPHATE) ...ETHYLENE GLYCOL (EDO): ETHYLENE GLYCOL WAS THE CRYOPROTECTANT GUANOSINE 5'-(TRIHYDROGEN DIPHOSPHATE), P'-D-MANNOPYRANOSYL ESTER (GDX): GDP-MANNOSE IS THE SUGAR DONOR SUBSTRATE FOR MGS CHLORIDE (CL): CHLORIDE OCCUPIES THE POSITION OF THE SUGAR ACCEPTOR OF MGS
配列の詳細
C-TERMINAL TRUNCATION OF LAST 15 RESIDUES. Q201 AND Q202 WERE BOTH MUTATED TO ALANINES FOR SURFACE ...C-TERMINAL TRUNCATION OF LAST 15 RESIDUES. Q201 AND Q202 WERE BOTH MUTATED TO ALANINES FOR SURFACE ENTROPY MINIMIZATION.
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 5.58 Å3/Da / 溶媒含有率: 78 % / 解説: NONE
結晶化
pH: 5 詳細: 4% V/V ETHYLENE GLYCOL, 0.1 M BIS-TRIS PROPANE, PH 5.5, 0.3 M MAGNESIUM FORMATE
解像度: 2.7→129.47 Å / Cor.coef. Fo:Fc: 0.94 / Cor.coef. Fo:Fc free: 0.923 / SU B: 7.432 / SU ML: 0.151 / 交差検証法: THROUGHOUT / ESU R: 0.276 / ESU R Free: 0.219 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. U VALUES REFINED INDIVIDUALLY
Rfactor
反射数
%反射
Selection details
Rfree
0.21878
2704
5.1 %
RANDOM
Rwork
0.19136
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obs
0.19279
47729
96.12 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.4 Å / 溶媒モデル: MASK