GAMMA-5R-HYDROXY-THERONINE (TH6): GAMMA-5R-HYDROXY-THERONINE WAS DIRECTLY LINKED TO PRS VIA CG ...GAMMA-5R-HYDROXY-THERONINE (TH6): GAMMA-5R-HYDROXY-THERONINE WAS DIRECTLY LINKED TO PRS VIA CG FORMING PLICAT L-THIOPROLINE (PRS): L-THIOPROLINE WAS DIRECTLY LINKED TO TH6 VIA CD FORMING PLICAT
配列の詳細
G1 WAS DELETED, Y2 WAS REPLACED BY NA8, FOR G10 A D-AMINO ACID WAS INTRODUCED (DAL), D17 AND G18 ...G1 WAS DELETED, Y2 WAS REPLACED BY NA8, FOR G10 A D-AMINO ACID WAS INTRODUCED (DAL), D17 AND G18 WERE REPLACED BY B-TURN MIMIC
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 2 Å3/Da / 溶媒含有率: 36.63 % / 解説: ONLY THE FOLDON PART OF THE STRUCTURE WAS USED
解像度: 1.06→26.02 Å / Cor.coef. Fo:Fc: 0.981 / Cor.coef. Fo:Fc free: 0.974 / SU B: 0.711 / SU ML: 0.017 / 交差検証法: THROUGHOUT / ESU R: 0.027 / ESU R Free: 0.029 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. U VALUES HAVE BEEN REFINED INDIVIDUALLY.
Rfactor
反射数
%反射
Selection details
Rfree
0.14024
1170
2 %
RANDOM
Rwork
0.10766
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obs
0.10832
56886
94.22 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK