SHEET THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN ... SHEET THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN THE SHEET RECORDS BELOW, TWO SHEETS ARE DEFINED.
ENGINEERED RESIDUE IN CHAIN A, THR 163 TO ASN ENGINEERED RESIDUE IN CHAIN A, ARG 164 TO GLN
配列の詳細
AMINO ACIDS 163 AND 164 TR REPLACED BY NQ
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実験情報
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実験
実験
手法: X線回折 / 使用した結晶の数: 1
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試料調製
結晶
マシュー密度: 2.37 Å3/Da / 溶媒含有率: 48 % / 解説: NONE
結晶化
pH: 8.5 詳細: 1 MICROLITER OF 15 MG/ML RECOMBINANT RAT CBG AND 1 MICROLITER OF RESERVOIR SOLUTION (30% (W/V) PEG 4000, 300 MM LI2SO4, 100 MM TRIS-HCL, PH 8.5) AGAINST 700 MICROLITER OF RESERVOIR SOLUTION
解像度: 1.93→37.42 Å / Cor.coef. Fo:Fc: 0.954 / Cor.coef. Fo:Fc free: 0.923 / SU B: 10.9 / SU ML: 0.154 / 交差検証法: THROUGHOUT / ESU R: 0.18 / ESU R Free: 0.171 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. ZERO OCCUPANCIES SET FOR SIDE CHAINS WHERE NO DENSITY WAS SEEN.
Rfactor
反射数
%反射
Selection details
Rfree
0.264
2328
8 %
RANDOM
Rwork
0.21
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obs
0.214
26770
100 %
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溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: BABINET MODEL WITH MASK