詳細 | Solution-ID | 内容 | 溶媒系 |
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1 | 1mM [U-98% 15N] MsPTH-1, 20mM sodium phosphate-2, 50mM sodium chloride-3, 1mM DTT-4, 1mM AEBSF protease inhibitor-5, 1% sodium azide-6, 93% H2O/7% D2O | 93% H2O/7% D2O2 | 1mM [U-98% 13C; U-98% 15N] MsPTH-7, 20mM sodium phosphate-8, 50mM sodium chloride-9, 1mM DTT-10, 1mM AEBSF protease inhibitor-11, 1% sodium azide-12, 93% H2O/7% D2O | 93% H2O/7% D2O3 | 0.9mM [U-98% 13C; U-98% 15N] MsPTH-13, 20mM sodium phosphate-14, 50mM sodium chloride-15, 1mM DTT-16, 1mM AEBSF protease inhibitor-17, 1% sodium azide-18, 100% D2O | 100% D2O | | |
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試料 | 濃度 (mg/ml) | 構成要素 | Isotopic labeling | Solution-ID |
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1 mMMsPTH-1 | [U-98% 15N] | 1 | 20 mMsodium phosphate-2 | | 1 | 50 mMsodium chloride-3 | | 1 | 1 mMDTT-4 | | 1 | 1 mMAEBSF protease inhibitor-5 | | 1 | 1 %sodium azide-6 | | 1 | 1 mMMsPTH-7 | [U-98% 13C; U-98% 15N] | 2 | 20 mMsodium phosphate-8 | | 2 | 50 mMsodium chloride-9 | | 2 | 1 mMDTT-10 | | 2 | 1 mMAEBSF protease inhibitor-11 | | 2 | 1 %sodium azide-12 | | 2 | 0.9 mMMsPTH-13 | [U-98% 13C; U-98% 15N] | 3 | 20 mMsodium phosphate-14 | | 3 | 50 mMsodium chloride-15 | | 3 | 1 mMDTT-16 | | 3 | 1 mMAEBSF protease inhibitor-17 | | 3 | 1 %sodium azide-18 | | 3 | | | | | | | | | | | | | | | | | | |
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試料状態 | イオン強度: 50 / pH: 6.5 / 圧: ambient / 温度: 303 K |
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