Mass: 18.015 Da / Num. of mol.: 348 / Source method: isolated from a natural source / Formula: H2O
Compound details
ENGINEERED RESIDUE IN CHAIN A, GLU 24 TO LYS ENGINEERED RESIDUE IN CHAIN B, GLU 24 TO LYS ...ENGINEERED RESIDUE IN CHAIN A, GLU 24 TO LYS ENGINEERED RESIDUE IN CHAIN B, GLU 24 TO LYS ENGINEERED RESIDUE IN CHAIN C, GLU 24 TO LYS ENGINEERED RESIDUE IN CHAIN D, GLU 24 TO LYS ENGINEERED RESIDUE IN CHAIN E, GLU 24 TO LYS
Sequence details
RESIDUE E24 HAS BEEN MUTATED TO K
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 1.75 Å3/Da / Density % sol: 29.72 %
Crystal grow
pH: 6.5 / Details: 10 % PEG 20000, 100 MM MES PH 6.5
Resolution: 1.85→42.91 Å / Cor.coef. Fo:Fc: 0.95 / Cor.coef. Fo:Fc free: 0.906 / SU B: 3.286 / SU ML: 0.102 / Cross valid method: THROUGHOUT / ESU R: 0.157 / ESU R Free: 0.161 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.253
1788
5 %
RANDOM
Rwork
0.183
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obs
0.186
34179
95.9 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.4 Å / Solvent model: MASK