ソフトウェア | 名称 | バージョン | 分類 |
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REFMAC | 5.1.24精密化 | AMoRE | | 位相決定 | |
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精密化 | 構造決定の手法: 分子置換 / 解像度: 2.3→20 Å / Cor.coef. Fo:Fc: 0.959 / Cor.coef. Fo:Fc free: 0.939 / SU B: 10.94 / SU ML: 0.138 / TLS residual ADP flag: LIKELY RESIDUAL / 交差検証法: THROUGHOUT / ESU R: 0.21 / ESU R Free: 0.186 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
| Rfactor | 反射数 | %反射 | Selection details |
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Rfree | 0.22835 | 2264 | 5.1 % | RANDOM |
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Rwork | 0.18481 | - | - | - |
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obs | 0.18699 | 42515 | 99.74 % | - |
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溶媒の処理 | イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: BABINET MODEL WITH MASK |
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原子変位パラメータ | Biso mean: 35.781 Å2
| Baniso -1 | Baniso -2 | Baniso -3 |
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1- | 0.48 Å2 | 0.24 Å2 | 0 Å2 |
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2- | - | 0.48 Å2 | 0 Å2 |
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3- | - | - | -0.72 Å2 |
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精密化ステップ | サイクル: LAST / 解像度: 2.3→20 Å
| タンパク質 | 核酸 | リガンド | 溶媒 | 全体 |
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原子数 | 4926 | 0 | 0 | 251 | 5177 |
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拘束条件 | Refine-ID | タイプ | Dev ideal | Dev ideal target | 数 |
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X-RAY DIFFRACTION | r_bond_refined_d0.029 | 0.021 | 5027 | X-RAY DIFFRACTION | r_bond_other_d0.006 | 0.02 | 4263 | X-RAY DIFFRACTION | r_angle_refined_deg2.1 | 1.921 | 6837 | X-RAY DIFFRACTION | r_angle_other_deg1.096 | 3 | 9895 | X-RAY DIFFRACTION | r_dihedral_angle_1_deg7.945 | 5 | 628 | X-RAY DIFFRACTION | r_dihedral_angle_2_deg35.324 | 24.196 | 255 | X-RAY DIFFRACTION | r_dihedral_angle_3_deg18.138 | 15 | 742 | X-RAY DIFFRACTION | r_dihedral_angle_4_deg22.612 | 15 | 26 | X-RAY DIFFRACTION | r_chiral_restr0.196 | 0.2 | 721 | X-RAY DIFFRACTION | r_gen_planes_refined0.011 | 0.02 | 5794 | X-RAY DIFFRACTION | r_gen_planes_other0.002 | 0.02 | 1090 | X-RAY DIFFRACTION | r_nbd_refined0.235 | 0.2 | 1089 | X-RAY DIFFRACTION | r_nbd_other0.232 | 0.2 | 4697 | X-RAY DIFFRACTION | r_nbtor_refined0.193 | 0.2 | 2427 | X-RAY DIFFRACTION | r_nbtor_other0.103 | 0.2 | 2698 | X-RAY DIFFRACTION | r_xyhbond_nbd_refined0.186 | 0.2 | 282 | X-RAY DIFFRACTION | r_xyhbond_nbd_other0.047 | 0.2 | 1 | X-RAY DIFFRACTION | r_metal_ion_refined | | | X-RAY DIFFRACTION | r_metal_ion_other | | | X-RAY DIFFRACTION | r_symmetry_vdw_refined0.282 | 0.2 | 23 | X-RAY DIFFRACTION | r_symmetry_vdw_other0.307 | 0.2 | 104 | X-RAY DIFFRACTION | r_symmetry_hbond_refined0.158 | 0.2 | 29 | X-RAY DIFFRACTION | r_symmetry_hbond_other | | | X-RAY DIFFRACTION | r_symmetry_metal_ion_refined | | | X-RAY DIFFRACTION | r_symmetry_metal_ion_other | | | X-RAY DIFFRACTION | r_mcbond_it1.709 | 1.5 | 3840 | X-RAY DIFFRACTION | r_mcbond_other0.347 | 1.5 | 1296 | X-RAY DIFFRACTION | r_mcangle_it1.857 | 2 | 5004 | X-RAY DIFFRACTION | r_scbond_it3.157 | 3 | 2286 | X-RAY DIFFRACTION | r_scangle_it4.319 | 4.5 | 1833 | X-RAY DIFFRACTION | r_rigid_bond_restr | | | X-RAY DIFFRACTION | r_sphericity_free | | | X-RAY DIFFRACTION | r_sphericity_bonded | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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LS精密化 シェル | 解像度: 2.3→2.359 Å / Total num. of bins used: 20
| Rfactor | 反射数 | %反射 |
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Rfree | 0.283 | 154 | - |
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Rwork | 0.237 | 3064 | - |
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obs | - | - | 99.94 % |
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精密化 TLS | 手法: refined / Refine-ID: X-RAY DIFFRACTION ID | L11 (°2) | L12 (°2) | L13 (°2) | L22 (°2) | L23 (°2) | L33 (°2) | S11 (Å °) | S12 (Å °) | S13 (Å °) | S21 (Å °) | S22 (Å °) | S23 (Å °) | S31 (Å °) | S32 (Å °) | S33 (Å °) | T11 (Å2) | T12 (Å2) | T13 (Å2) | T22 (Å2) | T23 (Å2) | T33 (Å2) | Origin x (Å) | Origin y (Å) | Origin z (Å) |
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1 | 0.7344 | 0.3548 | 0.4501 | 1.8321 | 0.5452 | 0.3405 | 0.0469 | 0.2994 | -0.3503 | -0.3194 | -0.0306 | -0.1512 | 0.097 | 0.0505 | -0.0163 | 0.1645 | -0.0575 | 0.0195 | 0.056 | -0.0701 | 0.077 | -46.262 | 19.7718 | 3.4631 | 2 | 1.117 | 1.6738 | -1.5375 | 6.158 | -0.3439 | 3.1689 | -0.0892 | -0.3138 | -0.2919 | 0.147 | 0.0427 | -0.0513 | 0.516 | 0.1888 | 0.0465 | 0.126 | -0.0094 | 0.0278 | 0.0586 | 0.0211 | 0.1342 | -41.7265 | 17.5599 | 24.8353 | 3 | 2.9981 | -0.1329 | -0.4392 | 0.8863 | 0.1666 | 0.0889 | -0.1026 | -0.1298 | -0.3188 | 0.091 | 0.0521 | 0.2388 | 0.4027 | -0.3325 | 0.0505 | 0.2808 | -0.1403 | 0.0646 | -0.0173 | -0.0612 | 0.1436 | -54.2207 | 0.9161 | 15.6213 | 4 | 3.2339 | -3.6366 | -4.4463 | 4.0896 | 5.0001 | 6.1132 | 0.7141 | -1.2975 | -1.2278 | 1.1001 | -1.0326 | -0.7526 | 1.0035 | -0.0796 | 0.3185 | 0.3649 | -0.2253 | -0.0075 | -0.0767 | -0.1146 | 0.1056 | -55.5275 | 0.6001 | 6.0876 | 5 | 4.853 | 3.2382 | -0.2567 | 4.3259 | -0.5182 | 8.8677 | 0.0348 | -0.3292 | -0.5679 | 0.523 | 0.0267 | 0.5324 | 0.5117 | -0.3087 | -0.0615 | 0.2608 | -0.0267 | 0.0787 | -0.0432 | -0.0452 | 0.1896 | -48.5467 | 3.7616 | 19.9291 | 6 | 1.0972 | -1.4294 | -1.2962 | 1.8907 | 1.4757 | 3.1243 | -0.0402 | -0.0178 | -0.2833 | -0.09 | 0.0552 | -0.0049 | 0.3823 | -0.0152 | -0.0151 | 0.1695 | -0.1092 | 0.0181 | 0.0466 | -0.0263 | 0.122 | -52.2652 | 14.7694 | 16.3163 | 7 | 3.1177 | -1.569 | 0.2245 | 4.2385 | 0.9488 | 1.7605 | 0.0357 | 0.016 | -0.5046 | 0.1644 | 0.0312 | 0.3884 | 0.3417 | -0.483 | -0.0669 | 0.1711 | -0.1891 | 0.0235 | 0.106 | 0.0429 | 0.1102 | -67.4925 | 10.9624 | 22.6434 | 8 | 5.5837 | 0.913 | 5.2742 | 2.0139 | -0.6669 | 6.2362 | -0.0666 | -0.1105 | -0.3322 | -0.1672 | 0.0929 | 0.1713 | 0.3852 | 0.0831 | -0.0263 | 0.2279 | -0.1363 | 0.0373 | 0.0536 | -0.0302 | 0.1202 | -57.2676 | 7.2025 | 14.9868 | 9 | 2.2949 | -1.6559 | -1.6569 | 7.2173 | -1.2452 | 2.1854 | 0.2909 | 0.3239 | -0.3482 | -0.3773 | -0.2696 | 0.2386 | 0.278 | -0.2873 | -0.0214 | 0.2083 | -0.1594 | -0.0803 | 0.097 | -0.0866 | 0.0732 | -61.4475 | 12.5301 | 5.0332 | 10 | 9.7188 | -3.3102 | -0.8032 | 6.2208 | 2.0871 | 0.7121 | 0.5491 | 0.9252 | 0.0783 | -0.8503 | -0.0288 | 0.5484 | -0.229 | -1.6799 | -0.5203 | -0.0994 | -0.6145 | 0.0022 | -0.1278 | 0.026 | -0.3835 | -66.3573 | 13.0702 | 17.8758 | 11 | 6.5278 | -2.2802 | 7.1339 | 9.0769 | -4.8398 | 8.462 | -0.2924 | -0.8096 | -0.1903 | 0.8509 | 0.5265 | 0.0219 | -0.4108 | -0.5776 | -0.2341 | 0.2012 | -0.0395 | 0.0663 | 0.1107 | 0.0764 | 0.1276 | -57.0833 | 12.4613 | 33.4085 | 12 | 1.28 | -0.0721 | -1.0479 | 0.8039 | 0.5288 | 4.7759 | 0.0249 | 0.0336 | -0.1081 | -0.0787 | 0.1399 | 0.2778 | 0.0442 | -0.391 | -0.1648 | 0.1265 | -0.1102 | -0.0237 | 0.0644 | -0.0076 | 0.0722 | -59.4141 | 20.9147 | 13.8355 | 13 | 1.8433 | -0.8844 | -0.591 | 1.7769 | -0.7044 | 1.78 | 0.0147 | 0.1275 | -0.1788 | -0.0245 | 0.0445 | 0.2094 | 0.1746 | -0.3407 | -0.0593 | 0.0721 | -0.0576 | -0.0116 | 0.0795 | -0.0295 | 0.0446 | -55.0818 | 32.318 | 13.1251 | 14 | 0.2068 | 0.5498 | -0.2672 | 1.9955 | -1.2915 | 0.9779 | -0.0247 | 0.2968 | 0.1336 | -0.1822 | -0.0597 | -0.1706 | -0.0952 | 0.0863 | 0.0844 | 0.1127 | -0.0173 | -0.0022 | 0.1155 | -0.0152 | 0.0789 | -41.4356 | 46.1921 | 2.2954 | 15 | 1.6483 | 0.9087 | 0.2543 | 0.5391 | 0.3535 | 1.2313 | 0.0681 | 0.2424 | 0.2651 | -0.2718 | -0.137 | -0.2126 | -0.1343 | 0.0629 | 0.0688 | 0.056 | -0.0094 | 0.0142 | 0.0892 | 0.0033 | 0.0547 | -35.505 | 55.8901 | 5.9182 | 16 | 0.635 | 0.0085 | -0.5082 | 0.2068 | -0.4171 | 1.2209 | 0.0011 | 0.0606 | -0.018 | -0.0486 | -0.0027 | -0.0378 | 0.0879 | -0.0347 | 0.0016 | 0.074 | -0.0131 | 0.0092 | 0.0619 | -0.0194 | 0.0454 | -44.1272 | 35.2145 | 12.2005 | 17 | 5.2593 | 12.2218 | 2.5971 | 28.9726 | 9.1561 | 18.3417 | -0.386 | -0.143 | -0.2513 | 0.4574 | 0.0414 | 0.8728 | 0.4258 | -0.5021 | 0.3446 | 0.1158 | -0.025 | 0.0452 | 0.0703 | -0.0708 | 0.0617 | -39.9533 | 24.9837 | -3.9993 | 18 | 2.0788 | -0.3185 | -0.5068 | 2.301 | 0.3309 | 0.152 | -0.0421 | 0.0781 | -0.3281 | -0.1127 | 0.0139 | -0.2115 | 0.3699 | 0.1178 | 0.0282 | 0.1437 | -0.0186 | 0.0432 | 0.0399 | -0.0236 | 0.0867 | -38.0469 | 22.8518 | 6.9509 | 19 | 0.5919 | 0.1217 | 0.0781 | 1.4377 | 1.041 | 1.7215 | -0.0286 | 0.151 | -0.2844 | -0.0499 | -0.0217 | -0.0513 | 0.3647 | 0.0015 | 0.0503 | 0.154 | -0.0105 | 0.0316 | 0.0291 | -0.0075 | 0.1172 | -38.4317 | 16.9906 | 16.866 | 20 | 1.3481 | 1.4419 | -0.6071 | 6.0142 | 1.124 | 3.8216 | -0.0345 | 0.031 | -0.4239 | 0.0157 | 0.1148 | -0.4552 | 0.2497 | 0.158 | -0.0802 | 0.2755 | -0.008 | 0.0619 | -0.0047 | -0.0594 | 0.1857 | -43.1782 | -2.3741 | 13.7373 | 21 | 2.6497 | -0.7586 | 1.9011 | 2.7417 | -0.8176 | 4.0135 | -0.0228 | 0.073 | -0.2973 | 0.093 | -0.081 | -0.1857 | 0.2405 | 0.3265 | 0.1039 | 0.0745 | 0.0247 | 0.0489 | 0.1037 | -0.0145 | 0.1523 | -20.4855 | 32.2568 | 19.2884 | 22 | 8.9989 | 2.8048 | -0.9144 | 1.6227 | 0.8057 | 1.6823 | -0.1255 | 0.4411 | -0.0124 | -0.0459 | -0.1012 | -0.1789 | -0.0908 | 0.1157 | 0.2267 | 0.1429 | 0.0855 | 0.1424 | 0.044 | -0.0843 | 0.1888 | -10.8183 | 27.8619 | 5.7811 | 23 | 0.109 | -0.8221 | -0.0778 | 6.2011 | 0.5868 | 0.0555 | 0.0323 | 0.1149 | -0.287 | -0.3712 | -0.0789 | -0.9256 | 0.2587 | 0.755 | 0.0466 | -0.0726 | 0.0432 | 0.105 | 0.2122 | 0.0218 | 0.2851 | 2.6452 | 37.8174 | 8.74 | 24 | 43.2893 | 1.8865 | -13.3404 | 8.2166 | 6.0834 | 13.5351 | 0.4969 | 1.0885 | 0.1794 | 0.369 | 0.0288 | -0.5062 | -0.4206 | 0.9766 | -0.5257 | 0.0537 | 0.0772 | -0.0346 | 0.127 | 0.1102 | 0.2411 | 1.6358 | 31.2421 | 17.8417 | 25 | 3.8674 | 1.169 | -4.2305 | 2.0412 | 1.2978 | 8.5603 | 0.0593 | 0.5665 | 0.0527 | -0.3399 | 0.1089 | -0.4714 | -0.3249 | 0.4135 | -0.1682 | 0.1177 | 0.0678 | 0.0909 | 0.1881 | -0.0366 | 0.2328 | -7.4979 | 31.1284 | 4.2289 | 26 | 0.9047 | 0.3879 | -0.5024 | 1.5097 | -0.4807 | 1.4006 | -0.0396 | 0.0367 | -0.1867 | -0.0873 | -0.029 | -0.2919 | 0.1301 | 0.3752 | 0.0686 | 0.0329 | 0.0169 | 0.0341 | 0.1286 | -0.0106 | 0.1088 | -9.0381 | 41.9793 | 10.7389 | 27 | 3.1635 | 0.0863 | -1.3554 | 1.9588 | -2.6201 | 5.8324 | -0.0057 | -0.1264 | -0.0631 | 0.2845 | -0.0617 | -0.2943 | -0.055 | 0.5185 | 0.0674 | -0.0046 | 0.0256 | -0.0297 | 0.2018 | -0.0014 | 0.1494 | -4.2022 | 42.3485 | 21.7909 | 28 | 1.5693 | 0.7943 | -1.8361 | 2.8837 | -1.2744 | 9.4513 | -0.2056 | 0.5737 | -0.2762 | -0.3745 | 0.1868 | 0.1787 | 0.4094 | 0.1289 | 0.0188 | 0.0341 | -0.0142 | 0.0517 | 0.1581 | -0.0301 | 0.1689 | -9.2597 | 47.2772 | 0.8922 | 29 | 1.4005 | 0.6964 | -0.1104 | 1.7283 | -1.9834 | 4.4957 | 0.0227 | -0.004 | 0.0069 | 0.0674 | 0.0175 | -0.1935 | -0.0926 | 0.2479 | -0.0402 | 0.0287 | 0.0118 | 0.0341 | 0.1108 | -0.0082 | 0.1233 | -14.8415 | 45.9496 | 16.5326 | 30 | 2.1822 | -0.7329 | -0.7071 | 1.4952 | 0.3034 | 2.0122 | -0.0188 | -0.095 | -0.0511 | 0.1294 | -0.0302 | -0.1171 | -0.0319 | 0.1029 | 0.049 | 0.0438 | -0.0109 | -0.0041 | 0.0525 | -0.0087 | 0.0685 | -27.6506 | 47.0002 | 21.8293 | 31 | 8.865 | -0.9993 | -4.288 | 5.2898 | 0.3704 | 9.362 | -0.1187 | -0.2605 | -0.0228 | 0.1949 | -0.0206 | 0.0545 | 0.0563 | -0.4341 | 0.1393 | 0.0771 | -0.0199 | 0.007 | 0.0915 | -0.001 | 0.0118 | -43.3411 | 35.5584 | 33.559 | 32 | 2.0532 | -0.8527 | -0.304 | 1.4834 | -0.1839 | 0.7264 | -0.0978 | -0.2047 | -0.03 | 0.3398 | 0.0414 | 0.1714 | 0.0565 | -0.2212 | 0.0564 | 0.0703 | -0.032 | 0.0123 | 0.0873 | -0.0071 | 0.0363 | -52.6705 | 38.8053 | 30.9951 | 33 | 5.3101 | 1.7877 | -8.5644 | 1.2973 | -2.9895 | 14.2547 | 0.0878 | -0.0822 | 0.1332 | 0.1876 | 0.085 | 0.0401 | 0.0904 | -0.1726 | -0.1728 | 0.0743 | -0.008 | -0.0097 | 0.0722 | -0.0005 | 0.0658 | -38.8703 | 41.1743 | 17.0137 | 34 | 1.5474 | 0.4994 | -1.3314 | 2.6548 | -2.8568 | 3.5079 | 0.0518 | -0.0133 | -0.1337 | -0.0145 | -0.0255 | -0.0279 | 0.2053 | -0.0072 | -0.0263 | 0.0681 | 0.0031 | -0.0061 | 0.053 | -0.0171 | 0.0595 | -31.1297 | 38.4231 | 21.4553 | 35 | 12.5773 | -1.5876 | -1.6883 | 6.6394 | -4.2638 | 3.3393 | -0.2488 | -0.4044 | 0.1755 | 0.397 | 0.3377 | -0.6197 | -0.034 | 0.3786 | -0.089 | 0.0851 | 0.0009 | -0.0317 | 0.04 | 0.0192 | 0.1049 | -25.1539 | 25.8949 | 31.996 | 36 | 1.2277 | 0.8629 | -0.5653 | 1.5395 | -0.643 | 0.8981 | 0.0119 | -0.1586 | -0.2826 | 0.0626 | -0.0214 | -0.2918 | 0.3119 | 0.1938 | 0.0094 | 0.1002 | 0.0225 | 0.0244 | 0.0446 | -0.0038 | 0.1194 | -25.8409 | 26.4302 | 21.6153 | 37 | 2.6957 | 0.0334 | 0.2069 | 4.6204 | -0.798 | 3.9695 | 0.0894 | 0.3609 | 0.0594 | -0.4334 | -0.1337 | -0.4268 | 0.1041 | 0.3239 | 0.0443 | 0.1129 | -0.0047 | 0.0486 | 0.0928 | -0.0367 | 0.0904 | -33.8379 | 36.467 | 1.6948 | 38 | 3.248 | 0.2584 | 2.2026 | 0.502 | 0.439 | 3.328 | 0.0788 | 0.0935 | -0.3563 | -0.0747 | -0.0256 | -0.2317 | 0.3822 | 0.2219 | -0.0532 | 0.105 | 0.0376 | 0.0669 | 0.0571 | -0.0143 | 0.1311 | -21.2782 | 25.0491 | 12.5208 | 39 | 0.4517 | -0.1688 | -0.7796 | 2.3281 | -1.5387 | 2.8239 | 0.015 | -0.2098 | -0.3448 | -0.1459 | -0.0202 | -0.6957 | 0.346 | 0.4426 | 0.0052 | 0.1192 | 0.0817 | 0.057 | 0.1165 | -0.0382 | 0.2666 | -4.7531 | 20.055 | 13.283 | 40 | 6.0924 | -0.6675 | -0.9067 | 1.1796 | -0.2347 | 3.561 | -0.2762 | -1.1371 | 0.4298 | -0.1493 | -0.0737 | 0.4662 | 0.1589 | -0.0844 | 0.35 | 0.096 | 0.1068 | 0.1546 | 0.0195 | -0.0798 | 0.1768 | -7.2636 | 22.3183 | 4.1069 |
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精密化 TLSグループ | ID | Refine-ID | Refine TLS-ID | Auth asym-ID | Label asym-ID | Auth seq-ID | Label seq-ID |
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1 | X-RAY DIFFRACTION | 1 | AA1 - 16 | 1 - 16 | 2 | X-RAY DIFFRACTION | 2 | AA17 - 26 | 17 - 26 | 3 | X-RAY DIFFRACTION | 3 | AA27 - 48 | 27 - 48 | 4 | X-RAY DIFFRACTION | 4 | AA49 - 52 | 49 - 52 | 5 | X-RAY DIFFRACTION | 5 | AA53 - 63 | 53 - 63 | 6 | X-RAY DIFFRACTION | 6 | AA64 - 86 | 64 - 86 | 7 | X-RAY DIFFRACTION | 7 | AA87 - 101 | 87 - 101 | 8 | X-RAY DIFFRACTION | 8 | AA102 - 111 | 102 - 111 | 9 | X-RAY DIFFRACTION | 9 | AA112 - 121 | 112 - 121 | 10 | X-RAY DIFFRACTION | 10 | AA122 - 129 | 122 - 129 | 11 | X-RAY DIFFRACTION | 11 | AA130 - 138 | 130 - 138 | 12 | X-RAY DIFFRACTION | 12 | AA139 - 163 | 139 - 163 | 13 | X-RAY DIFFRACTION | 13 | AA164 - 186 | 164 - 186 | 14 | X-RAY DIFFRACTION | 14 | AA187 - 197 | 187 - 197 | 15 | X-RAY DIFFRACTION | 15 | AA198 - 210 | 198 - 210 | 16 | X-RAY DIFFRACTION | 16 | AA211 - 236 | 211 - 236 | 17 | X-RAY DIFFRACTION | 17 | AA237 - 240 | 237 - 240 | 18 | X-RAY DIFFRACTION | 18 | AA241 - 257 | 241 - 257 | 19 | X-RAY DIFFRACTION | 19 | AA258 - 304 | 258 - 304 | 20 | X-RAY DIFFRACTION | 20 | AA305 - 316 | 305 - 316 | 21 | X-RAY DIFFRACTION | 21 | BB1 - 22 | 1 - 22 | 22 | X-RAY DIFFRACTION | 22 | BB23 - 35 | 23 - 35 | 23 | X-RAY DIFFRACTION | 23 | BB36 - 48 | 36 - 48 | 24 | X-RAY DIFFRACTION | 24 | BB49 - 52 | 49 - 52 | 25 | X-RAY DIFFRACTION | 25 | BB53 - 63 | 53 - 63 | 26 | X-RAY DIFFRACTION | 26 | BB64 - 109 | 64 - 109 | 27 | X-RAY DIFFRACTION | 27 | BB110 - 124 | 110 - 124 | 28 | X-RAY DIFFRACTION | 28 | BB125 - 136 | 125 - 136 | 29 | X-RAY DIFFRACTION | 29 | BB137 - 163 | 137 - 163 | 30 | X-RAY DIFFRACTION | 30 | BB164 - 189 | 164 - 189 | 31 | X-RAY DIFFRACTION | 31 | BB190 - 195 | 190 - 195 | 32 | X-RAY DIFFRACTION | 32 | BB196 - 213 | 196 - 213 | 33 | X-RAY DIFFRACTION | 33 | BB214 - 221 | 214 - 221 | 34 | X-RAY DIFFRACTION | 34 | BB222 - 236 | 222 - 236 | 35 | X-RAY DIFFRACTION | 35 | BB237 - 240 | 237 - 240 | |
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