Mass: 18.015 Da / Num. of mol.: 164 / Source method: isolated from a natural source / Formula: H2O
Compound details
CONVERTS BY REDUCTION ARSENATE AS(V) INTO ARSENITE AS(III) AND DEPHOSPHORYLATES TYROSINE ...CONVERTS BY REDUCTION ARSENATE AS(V) INTO ARSENITE AS(III) AND DEPHOSPHORYLATES TYROSINE PHOSPHORYLATED PROTEINS, LOW-MW ARYL PHOSPHATES AND ACYL PHOSPHATES. ENGINEERED RESIDUE IN CHAIN A, HIS 62 TO GLN
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 1.69 Å3/Da / Density % sol: 26.52 %
Crystal grow
pH: 8 Details: 100 MM TRIS/HCL, PH 8.0, 10 MM DTT, 42.5 % (WT/VOL) POLYETHYLENE GLYCOL 4000
Resolution: 1.5→14.9 Å / Cor.coef. Fo:Fc: 0.958 / Cor.coef. Fo:Fc free: 0.942 / SU B: 1.253 / SU ML: 0.049 / Cross valid method: THROUGHOUT / ESU R: 0.096 / ESU R Free: 0.095 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.218
847
5.1 %
RANDOM
Rwork
0.184
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obs
0.185
15786
88.6 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK