THE BIOLOGICAL UNIT OF ARABIDOPSIS THALIANA THREONINESYNTHASE (HOMODIMER) IN COMPLEX WITH SAM IS FORMED BY TWOASYMETRIC MONOMERS. IN ONE MONOMER THE ACTIVE SITECORRESPONDS TO AN INACTIVE FORM WHEREAS IN THE OTHERMONOMER, THE ACTIVE SITE CORRESPONDS TO AN ACTIVE FORM WITHA STANDARD PLP ORIENTATION FOR A TYPE II FAMILY PLPENZYMES.
解像度: 2.6→29.89 Å / Cor.coef. Fo:Fc: 0.945 / Cor.coef. Fo:Fc free: 0.922 / SU B: 25.549 / SU ML: 0.272 / TLS residual ADP flag: LIKELY RESIDUAL / 交差検証法: THROUGHOUT / ESU R: 0.812 / ESU R Free: 0.311 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. RESIDUES 1-35 AND 480-486 ARE DISORDERED IN MONOMERS A, C AND F RESIDUS 1-34, 344-362 AND 482-486 ARE DISORDERED IN MONOMERS B, D AND E.
Rfactor
反射数
%反射
Selection details
Rfree
0.248
4904
5 %
RANDOM
Rwork
0.206
-
-
-
obs
0.208
93254
100 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK