Mass: 104.061 Da / Num. of mol.: 6 / Source method: obtained synthetically / Formula: C3H4O4
Sequence details
THE SIX RESIDUE HIS TAG (RESIDUES X893-X898) WERE NOT SEEN IN THE DENSITY. THE UNIPROT ENTRY ...THE SIX RESIDUE HIS TAG (RESIDUES X893-X898) WERE NOT SEEN IN THE DENSITY. THE UNIPROT ENTRY INCLUDES REFERENCES DETAILING SEVERAL SEQUENCE CONFLICTS.
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 2.56 Å3/Da / Density % sol: 51.64 %
Resolution: 3.3→69.01 Å / Cor.coef. Fo:Fc: 0.881 / Cor.coef. Fo:Fc free: 0.84 / Cross valid method: THROUGHOUT / ESU R Free: 0.81 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS.
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.327
578
5 %
RANDOM
Rwork
0.301
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obs
0.302
11046
93.8 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK