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Open data
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Basic information
Entry | Database: PDB / ID: 266d | ||||||||||||||||||
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Title | STRUCTURAL STUDIES ON NUCLEIC ACIDS | ||||||||||||||||||
![]() | DNA (5'-D(*![]() DNA / B-DNA / DOUBLE HELIX / MODIFIED | Function / homology | DNA / DNA (> 10) | ![]() Method | ![]() ![]() ![]() Partridge, B.L. / Salisbury, S.A. | ![]() #1: ![]() Title: Structural Studies on Nucleic Acids Authors: Partridge, B.L. History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 28.2 KB | Display | ![]() |
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PDB format | ![]() | 16.5 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Summary document | ![]() | 376.8 KB | Display | ![]() |
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Full document | ![]() | 406 KB | Display | |
Data in XML | ![]() | 8.1 KB | Display | |
Data in CIF | ![]() | 9.5 KB | Display | |
Arichive directory | ![]() ![]() | HTTPS FTP |
-Related structure data
Related structure data | |
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Similar structure data |
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Links
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Assembly
Deposited unit | ![]()
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Unit cell |
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Components
#1: DNA chain | Mass: 3677.419 Da / Num. of mol.: 2 / Source method: obtained synthetically #2: Chemical | ChemComp-MG / | #3: Water | ChemComp-HOH / | |
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-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 2.32 Å3/Da / Density % sol: 47.02 % | ||||||||||||
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Crystal grow | pH: 7.1 / Details: pH 7.10 | ||||||||||||
Components of the solutions |
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-Data collection
Diffraction | Mean temperature: 277 K |
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Diffraction source | Source: ![]() |
Detector | Type: RIGAKU RAXIS IIC / Detector: IMAGE PLATE / Date: Mar 22, 1994 |
Radiation | Monochromator: GRAPHITE / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Relative weight: 1 |
Reflection | Resolution: 2.03→40.8 Å / Num. obs: 12395 / Rmerge(I) obs: 0.0677 |
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Processing
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Refinement | Method to determine structure: ![]() Details: STANDARD R-FACTOR = 16.6% ERROR R-FACTOR = 6.6% WEIGHTED R-FACTOR = 15.2% NUMBER OF REFLECTIONS INCLUDED = 12395 AVERAGE |FO-FC| DISCREPANCY = 16.06 AVERAGE WEIGHTED |FO-FC| DISCREPANCY = 0. ...Details: STANDARD R-FACTOR = 16.6% ERROR R-FACTOR = 6.6% WEIGHTED R-FACTOR = 15.2% NUMBER OF REFLECTIONS INCLUDED = 12395 AVERAGE |FO-FC| DISCREPANCY = 16.06 AVERAGE WEIGHTED |FO-FC| DISCREPANCY = 0.17 CORRELATION COEFFICIENT = 98.8% RESOLUTION BREAKDOWN "ALL" R FACTOR = 15.0%
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Refinement step | Cycle: LAST / Highest resolution: 2.03 Å
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Refine LS restraints |
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